546-0335/01 – Instrumental Methods of Analysis I (IMA I)
| Gurantor department | Department of Environmental Engineering | Credits | 9 |
| Subject guarantor | doc. Mgr. Eva Pertile, Ph.D. | Subject version guarantor | doc. Mgr. Eva Pertile, Ph.D. |
| Study level | undergraduate or graduate | Requirement | Compulsory |
| Year | 2 | Semester | summer |
| | Study language | Czech |
| Year of introduction | 2005/2006 | Year of cancellation | 2007/2008 |
| Intended for the faculties | HGF | Intended for study types | Bachelor |
Subject aims expressed by acquired skills and competences
The main objective of lectures is to create a compact picture about modern analytical chemistry. Lectures are conceived so that students get an overview of general parts of analytical chemistry, which serves as a necessity to understand the laws of chemistry and reaction analysis and then is followed with an overview of various groups of practical activities, leading to the determination of the reference analyte.
Teaching methods
Lectures
Experimental work in labs
Other activities
Summary
The aim of the course is to broaden and deepen knowledge of chemical laboratory techniques including gaining practical skills. The aim of the course is to deepen students' readiness to solve analytic problems by selected instrumental methods. Provide an overview of selected analytical methods and procedures used to analyze real environmental samples and chemometric evaluation of analytical results.
Compulsory literature:
Recommended literature:
Way of continuous check of knowledge in the course of semester
Lecture and exercising are conceived as a block course for combination form of studies.
E-learning
Other requirements
Prerequisities
Subject has no prerequisities.
Co-requisities
Subject has no co-requisities.
Subject syllabus:
1. Determination problems. Basic notions. Processes data acquisition. Basic classification of analytical methods.
2. Basic units of concentration and calculations. Type of interaction. Chemical balances in analytical chemistry. Classification of analytical reaction.
3. Case of analyses – common tissue: exercise formulation and proposal; sampling, sample adjustment before analysis; separative and concentration steps; measurement; measurement interpretation and formulation of results analyses; activities proposal resulting from acquired dates.
4. Sampling, common sampling fundamentals. Standard operational procedure for sampling; system QA/QC.
5. Basic sampling characteristics for abiotic and biotic matrixs. Atmosphere sampling, including passive sampling.
6. Sampling drinking and surface waters; sediment sampling; sampling underground and outlet waters; sampling sludge from sewage disposal plant; sampling soil sphere.
7. Biotic matrixs sampling. Wastes sampling.
8. Sample adjustment before analysis. Analytical method NDRO. Destructive analytical methods: Samle solution and analysis, mineralization.
9. Separative and concentration steps: elimination interference with chemical methods (masking) and physical speparation. Separative methods: dividing according to axiom and according to experimental ordering. Extraction. Separation on ion exchanger. Influence separative of the process.
10. Classification of analytical results and techniques and formulation results of analyses. A ctivities proposal implicit from gained data. GLP. Chemometric principles.
11. Principles of qualitative analyses: classic system of dividing cation – hydrogen sulphide system, analytical anion classes. Next criteria at anion determination. Heteroatoms verification in organic matter.
12. View of basic analytical methods and their common property: method based on weighing, on measuring of volume. Gravimetric analysis: axioms, analytical usage. Basic steps of analyses: sample adjustment, removing, washinh process and filtration, drying, coagulation weighing,concentration calculation .
13. Quantitative chemical analysis. Volumetric analysis (volumetry): common procedure of determination, determination final point of titration, titration curve, calculation of sample content from titrating data. Types of volumetric determination and their application: acidobasic titration, coagulative titration, complex-forming agent titration, redox titration. Axioms, analytical usage.
14. Developments in analytical chemistry - mobile analytics.
Conditions for subject completion
Occurrence in study plans
Occurrence in special blocks
Assessment of instruction
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