546-0335/01 – Instrumental Methods of Analysis I (IMA I)

Gurantor departmentDepartment of Environmental EngineeringCredits9
Subject guarantordoc. Mgr. Eva Pertile, Ph.D.Subject version guarantordoc. Mgr. Eva Pertile, Ph.D.
Study levelundergraduate or graduateRequirementCompulsory
Year2Semestersummer
Study languageCzech
Year of introduction2005/2006Year of cancellation2007/2008
Intended for the facultiesHGFIntended for study typesBachelor
Instruction secured by
LoginNameTuitorTeacher giving lectures
PER34 doc. Mgr. Eva Pertile, Ph.D.
Extent of instruction for forms of study
Form of studyWay of compl.Extent
Part-time Credit and Examination 12+8

Subject aims expressed by acquired skills and competences

The main objective of lectures is to create a compact picture about modern analytical chemistry. Lectures are conceived so that students get an overview of general parts of analytical chemistry, which serves as a necessity to understand the laws of chemistry and reaction analysis and then is followed with an overview of various groups of practical activities, leading to the determination of the reference analyte.

Teaching methods

Lectures
Experimental work in labs
Other activities

Summary

The aim of the course is to broaden and deepen knowledge of chemical laboratory techniques including gaining practical skills. The aim of the course is to deepen students' readiness to solve analytic problems by selected instrumental methods. Provide an overview of selected analytical methods and procedures used to analyze real environmental samples and chemometric evaluation of analytical results.

Compulsory literature:

PERTILE, E. Instrumental Methods of Analysis. Ostrava: Vysoká škola báňská - Technická univerzita Ostrava, 2017. ISBN 978-80-248-4124-3. CHANG R. Chemistry. 10th Edition. McGraw-Hill: New York, 2010. 1170 p. Available from: https://archive.org/details/Chemistry_10th_Edition_Raymond_Chang. GRANGER, B. New developments in analytical chemistry research. New York: Nova Publishers, 2015. Chemistry research and applications series. ISBN 1634634276. ANDRADE G., J. M. A. CARLOSENA ZUBIETA, M. P. GÓMEZ-CARRACEDO, M. Á. MAESTRO SAAVEDRA, M. C. PRIETO-BLANCO and R. M. SOTO-FERREIRO. Problems of instrumental analytical chemistry: a hands-on guide. New Jersey: World Scientific, 2017. Essential textbooks in chemistry. ISBN 978-1-78634-179-2.

Recommended literature:

Trends in Environmental Analytical Chemistry [online]. 2018, 17-20(4). ISSN 2214-1588. Dostupné z: https://www.sciencedirect.com/journal/trends-in-environmental-analytical-chemistry. HANRAHAN, G. Key concepts in environmental chemistry. Burlington: Elsevier Science, 2011. ISBN 9780080961705. Dostupné z: http://booksite.elsevier.com/samplechapters/9780123749932/Front_Matter.pdf. AHUJA, S. Chemistry and water: the science behind sustaining the world's most crucial resource. Amsterdam: Elsevier, 2017. ISBN 978-0-12-809330-6. Dostupné z: https://www.sciencedirect.com/science/book/9780128093306. PETROZZI, S. Practical instrumental analysis: methods, quality assurance and laboratory management. Weinheim: Wiley-VCH, c2013. ISBN 978-3-527-32951-9.

Way of continuous check of knowledge in the course of semester

Lecture and exercising are conceived as a block course for combination form of studies.

E-learning

Další požadavky na studenta

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

1. Determination problems. Basic notions. Processes data acquisition. Basic classification of analytical methods. 2. Basic units of concentration and calculations. Type of interaction. Chemical balances in analytical chemistry. Classification of analytical reaction. 3. Case of analyses – common tissue: exercise formulation and proposal; sampling, sample adjustment before analysis; separative and concentration steps; measurement; measurement interpretation and formulation of results analyses; activities proposal resulting from acquired dates. 4. Sampling, common sampling fundamentals. Standard operational procedure for sampling; system QA/QC. 5. Basic sampling characteristics for abiotic and biotic matrixs. Atmosphere sampling, including passive sampling. 6. Sampling drinking and surface waters; sediment sampling; sampling underground and outlet waters; sampling sludge from sewage disposal plant; sampling soil sphere. 7. Biotic matrixs sampling. Wastes sampling. 8. Sample adjustment before analysis. Analytical method NDRO. Destructive analytical methods: Samle solution and analysis, mineralization. 9. Separative and concentration steps: elimination interference with chemical methods (masking) and physical speparation. Separative methods: dividing according to axiom and according to experimental ordering. Extraction. Separation on ion exchanger. Influence separative of the process. 10. Classification of analytical results and techniques and formulation results of analyses. A ctivities proposal implicit from gained data. GLP. Chemometric principles. 11. Principles of qualitative analyses: classic system of dividing cation – hydrogen sulphide system, analytical anion classes. Next criteria at anion determination. Heteroatoms verification in organic matter. 12. View of basic analytical methods and their common property: method based on weighing, on measuring of volume. Gravimetric analysis: axioms, analytical usage. Basic steps of analyses: sample adjustment, removing, washinh process and filtration, drying, coagulation weighing,concentration calculation . 13. Quantitative chemical analysis. Volumetric analysis (volumetry): common procedure of determination, determination final point of titration, titration curve, calculation of sample content from titrating data. Types of volumetric determination and their application: acidobasic titration, coagulative titration, complex-forming agent titration, redox titration. Axioms, analytical usage. 14. Developments in analytical chemistry - mobile analytics.

Conditions for subject completion

Part-time form (validity from: 1960/1961 Summer semester, validity until: 2008/2009 Summer semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of points
Exercises evaluation and Examination Credit and Examination 100 (100) 51
        Exercises evaluation Credit 45 (45) 0
                Project Project 45  0
        Examination Examination 55 (55) 0
                Written examination Written examination 25  0
                Oral Oral examination 30  0
Mandatory attendence parzicipation:

Show history

Occurrence in study plans

Academic yearProgrammeField of studySpec.ZaměřeníFormStudy language Tut. centreYearWSType of duty
2006/2007 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Ostrava 2 Compulsory study plan
2006/2007 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Most 2 Compulsory study plan
2005/2006 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Ostrava 2 Compulsory study plan
2005/2006 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Most 2 Compulsory study plan

Occurrence in special blocks

Block nameAcademic yearForm of studyStudy language YearWSType of blockBlock owner