546-0354/01 – Instrumental Methods of Analysis (IMA)
Gurantor department | Department of Environmental Engineering | Credits | 8 |
Subject guarantor | doc. Mgr. Eva Pertile, Ph.D. | Subject version guarantor | doc. Mgr. Eva Pertile, Ph.D. |
Study level | undergraduate or graduate | Requirement | Compulsory |
Year | 2 | Semester | winter |
| | Study language | Czech |
Year of introduction | 2006/2007 | Year of cancellation | 2008/2009 |
Intended for the faculties | HGF | Intended for study types | Bachelor |
Subject aims expressed by acquired skills and competences
Obtaining basic knowledge not only about environmental sampling in relation to its share in the overall uncertainty of environmental analyzes but also in instrumental analytical methods. This will increase student readiness to solve analytic problems by selected instrumental methods.
Obtaining the competence to work in an analytical laboratory with basic instrumental equipment, the ability to present and evaluate the results, to learn the correct principles of working with the sample.
Teaching methods
Lectures
Experimental work in labs
Terrain work
Other activities
Summary
The lecture provides information about selected modern instrumental methods of research and monitoring of the environment, its use and application. During the lectures, students will get acquainted with the principles of analytical methods that are commonly used in control and development analytical laboratories.
Compulsory literature:
Recommended literature:
Way of continuous check of knowledge in the course of semester
The every laboratory starts with 5-minute 6-question test, to prove that student read the manual and is able to work safely and purposefully. The 3 questions need to be answered correctly to be allowed to work. If not the test is classified “0b”. Every work is classified after delivering of report or the not classified if report is not delivered or delivered late.
E-learning
Other requirements
Prerequisities
Subject has no prerequisities.
Co-requisities
Subject has no co-requisities.
Subject syllabus:
1. Determination problems. Basic notions. Processes data acquisition. Basic classification of analytical methods.
2. Basic units of concentration and calculations. Type of interaction. Chemical balances in analytical chemistry. Classification of analytical reaction.
3. Case of analyses – common tissue: exercise formulation and proposal; sampling, sample adjustment before analysis; separative and concentration steps; measurement; measurement interpretation and formulation of results analyses; activities proposal resulting from acquired dates.
4. Sampling, common sampling fundamentals. Standard operational procedure for sampling; system QA/QC.
5. Basic sampling characteristics for abiotic and biotic matrixs. Atmosphere sampling, including passive sampling.
6. Sampling drinking and surface waters; sediment sampling; sampling underground and outlet waters; sampling sludge from sewage disposal plant; sampling soil sphere.
7. Biotic matrixs sampling. Wastes sampling.
8. Sample adjustment before analysis. Analytical method NDRO. Destructive analytical methods: Samle solution and analysis, mineralization.
9. Separative and concentration steps: elimination interference with chemical methods (masking) and physical speparation. Separative methods: dividing according to axiom and according to experimental ordering. Extraction. Separation on ion exchanger. Influence separative of the process.
10. Classification of analytical results and techniques and formulation results of analyses. A ctivities proposal implicit from gained data. GLP. Chemometric principles.
11. Principles of qualitative analyses: classic system of dividing cation – hydrogen sulphide system, analytical anion classes. Next criteria at anion determination. Heteroatoms verification in organic matter.
12. View of basic analytical methods and their common property: method based on weighing, on measuring of volume. Gravimetric analysis: axioms, analytical usage. Basic steps of analyses: sample adjustment, removing, washinh process and filtration, drying, coagulation weighing,concentration calculation .
13. Quantitative chemical analysis. Volumetric analysis (volumetry): common procedure of determination, determination final point of titration, titration curve, calculation of sample content from titrating data. Types of volumetric determination and their application: acidobasic titration, coagulative titration, complex-forming agent titration, redox titration. Axioms, analytical usage.
14. Developments in analytical chemistry - mobile analytics.
Conditions for subject completion
Occurrence in study plans
Occurrence in special blocks
Assessment of instruction
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