546-0354/02 – Instrumental Methods of Analysis (IMA)

Gurantor departmentDepartment of Environmental EngineeringCredits6
Subject guarantordoc. Mgr. Eva Pertile, Ph.D.Subject version guarantordoc. Mgr. Eva Pertile, Ph.D.
Study levelundergraduate or graduateRequirementCompulsory
Year2Semestersummer
Study languageCzech
Year of introduction2006/2007Year of cancellation2008/2009
Intended for the facultiesHGFIntended for study typesBachelor
Instruction secured by
LoginNameTuitorTeacher giving lectures
NEZ022 Ing. Lucie Čablíková
PER34 doc. Mgr. Eva Pertile, Ph.D.
STE68 Ing. Radka Wolfová, Ph.D.
Extent of instruction for forms of study
Form of studyWay of compl.Extent
Full-time Credit and Examination 1+4

Subject aims expressed by acquired skills and competences

Obtaining basic knowledge not only about environmental sampling in relation to its share in the overall uncertainty of environmental analyzes but also in instrumental analytical methods. This will increase student readiness to solve analytic problems by selected instrumental methods. Obtaining the competence to work in an analytical laboratory with basic instrumental equipment, the ability to present and evaluate the results, to learn the correct principles of working with the sample.

Teaching methods

Lectures
Experimental work in labs
Terrain work
Other activities

Summary

The lecture provides information about selected modern instrumental methods of research and monitoring of the environment, its use and application. During the lectures, students will get acquainted with the principles of analytical methods that are commonly used in control and development analytical laboratories.

Compulsory literature:

CHANG R.: Chemistry. 10th Edition. McGraw-Hill: New York, 2010. 1170 p. Dostupné z: https://archive.org/details/Chemistry_10th_Edition_Raymond_Chang PERTILE, E. Instrumental Methods of Analysis. Ostrava: Vysoká škola báňská - Technická univerzita Ostrava, 2017. ISBN 978-80-248-4124-3

Recommended literature:

ROUESSAC Francis and ROUESSAC, Annick: Chemical Analysis Modern Instrumentation Methods and Techniques. March 2007. 600 pp. ISBN: 978-0-470-85903-2 NOLLET M., L., Chromatographic Analysis of the Environment, Chromatographic Science Series, Volume 93, 1297 s. 2006, ISBN 0-8247-2629-4

Way of continuous check of knowledge in the course of semester

The every laboratory starts with 5-minute 6-question test, to prove that student read the manual and is able to work safely and purposefully. The 3 questions need to be answered correctly to be allowed to work. If not the test is classified “0b”. Every work is classified after delivering of report or the not classified if report is not delivered or delivered late.

E-learning

Other requirements

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

1. Problems delimitation. Basic concepts. Processes obtaining information. Analytical methods absolute and comparative. Calibration methods. Developments in instrumentation methods of analyses. 2. - 3. Results classification of analyses and way their explication. Statistical interpretation of analytical results. Referential material, circular test. Principles of chemometric accesses and methods. Testing of metrological results properties. 4. Fundamental principles of electroanalytical methods and their classification. Theoretic principles. 5. Electroanalytical methods: methods based on measuring of potential (equilibrium potentiometry, potentiometric titrations). Axioms, instrumentation, utilization, advantages and disavantages. 6. Electroanalytical methods: methods based on current (voltammetry and polarography, coulometry, electrogravimetry) and conductivity (conductometry). Axioms, instrumentation, utilization, advantages and disavantages. 7. Optical analytical methods: theoretic principles. Optical spectral apparatus. Methods without exchange of energy (refractometry, polarimetry, nephelometry). Axioms, instrumentation, utilization, advantages and disavantages. 8. - 9. Emissive atomic spectral frequency bands. Flame photometer photometry. Atomic absorptive spectrometric: UV/Vis spectrometric, luminescent analysis. Principles theory, instrumentation, qualitative and quantitative aspects, application, analytical utilization. Automatic analyzers with optical detection: FIA, CFA. 10. Infra - red spectrometric - method axiom, instrumentation, analytical utilization. Raman spectra - method axiom , analytical utilization. 11. Separative and concentration steps: theory. Separative methods:classification according to axiom and according to experimental ordering, operation separative of the process. Extraction. 12. Diaphragm separation. Mass spectrometry. Bases theory, instrumentation, qualitative and quantitative aspects, application. 13. Chromatographic methods. Planar chromatography: Chromatography on thin layer, bases theory, instrumentation, qualitative and quantitative aspects, application. 11. Column chromatography: Liquid chromatography. Gas chromatography. Theory, bases instrumentation, qualitative and quantitative characteristics, analytical utilization. 14. Electromigration methods: theory, zonal and capillary electrophoresis, isotachophoresis. Bases instrumentation, qualitative and quantitative characteristics, analytical utilization.

Conditions for subject completion

Full-time form (validity from: 1960/1961 Summer semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of pointsMax. počet pokusů
Exercises evaluation and Examination Credit and Examination 100 (100) 51 3
        Exercises evaluation Credit 45 (45) 0 3
                Project Project 30  0 3
                Written exam Written test 15  0 3
        Examination Examination 55 (55) 0 3
                Written examination Written examination 25  0 3
                Oral Oral examination 30  0 3
Mandatory attendence participation:

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Conditions for subject completion and attendance at the exercises within ISP:

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Occurrence in study plans

Academic yearProgrammeBranch/spec.Spec.ZaměřeníFormStudy language Tut. centreYearWSType of duty
2008/2009 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal P Czech Ostrava 2 Compulsory study plan
2007/2008 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal P Czech Ostrava 2 Compulsory study plan
2006/2007 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal P Czech Ostrava 2 Compulsory study plan

Occurrence in special blocks

Block nameAcademic yearForm of studyStudy language YearWSType of blockBlock owner

Assessment of instruction

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