546-0354/08 – Instrumental Methods of Analysis (IMA)

Gurantor departmentDepartment of Environmental EngineeringCredits5
Subject guarantordoc. Mgr. Eva Pertile, Ph.D.Subject version guarantordoc. Mgr. Eva Pertile, Ph.D.
Study levelundergraduate or graduateRequirementCompulsory
Year3Semesterwinter
Study languageCzech
Year of introduction2022/2023Year of cancellation
Intended for the facultiesHGFIntended for study typesBachelor
Instruction secured by
LoginNameTuitorTeacher giving lectures
PER34 doc. Mgr. Eva Pertile, Ph.D.
SYR0013 Ing. Lucie Syrová
Extent of instruction for forms of study
Form of studyWay of compl.Extent
Full-time Credit and Examination 2+3
Part-time Credit and Examination 8+12

Subject aims expressed by acquired skills and competences

Obtaining basic knowledge not only about environmental sampling in relation to its share in the overall uncertainty of environmental analyzes but also in instrumental analytical methods. This will increase student readiness to solve analytic problems by selected instrumental methods. Obtaining the competence to work in an analytical laboratory with basic instrumental equipment, the ability to present and evaluate the results, to learn the correct principles of working with the sample.

Teaching methods

Lectures
Experimental work in labs
Terrain work
Other activities

Summary

The lecture provides information about selected modern instrumental methods of research and monitoring of the environment, its use and application. During the lectures, students will get acquainted with the principles of analytical methods that are commonly used in control and development analytical laboratories.

Compulsory literature:

CHANG R.: Chemistry. 10th Edition. McGraw-Hill: New York, 2010. 1170 p. Dostupné z: https://archive.org/details/Chemistry_10th_Edition_Raymond_Chang PERTILE, E. Instrumental Methods of Analysis. Ostrava: Vysoká škola báňská - Technická univerzita Ostrava, 2017. ISBN 978-80-248-4124-3

Recommended literature:

ROUESSAC Francis and ROUESSAC, Annick: Chemical Analysis Modern Instrumentation Methods and Techniques. March 2007. 600 pp. ISBN: 978-0-470-85903-2 NOLLET M., L., Chromatographic Analysis of the Environment, Chromatographic Science Series, Volume 93, 1297 s. 2006, ISBN 0-8247-2629-4

Way of continuous check of knowledge in the course of semester

Student knowledge is verified in written form, emphasis is given to understanding the subject and applying theoretical knowledge to solving practical problems. The evaluation also includes collective evaluation and self-assessment. An active assessment of the students is also included in the class. The course is completed by a credit and a combined exam (written and oral).

E-learning

Other requirements

Active participation in the exercises, demonstrated the successful processing of subtasks, entered continuously in the semester.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

1. Defining the issue. Information retrieval processes. Evaluation of analytical results and procedures, expression of analysis results. Statistical processing of results. Proposal of activities resulting from the obtained data. GLP principles. 2. Sampling, general principles of the source of errors. Standard Operating Procedures for Sampling; QA / QC system. 3. Sample preparation before analysis. Non-destructive methods. Destructive methods. Separation and concentration steps. 4. Basics of qualitative analysis 5. Overview of basic analytical methods and their general properties: methods based on weighing, on volume measurement. Principles of individual methods; instrumentation; applications in the analysis of environmental components; Advantages, disadvantages. 6. Introduction to instrumental methods. Absolute and comparative analytical methods. Rapid analytical methods - screening. Intended use. Advantages, disadvantages. Calibration methods. 7. Electroanalytical methods based on voltage and current measurements. Applications in the analysis of environmental components; Advantages, disadvantages. 8. Overview of separation methods: application in the analysis of environmental components; Advantages, disadvantages. 9. Column chromatography: GC + HPLC. New trends: UHPLC, GC / MS, HPLC / MS. Applications in the analysis of environmental components; Advantages, disadvantages. 10. Electrophoresis. Mass spectrometry. Applications in the analysis of environmental components; Advantages, disadvantages. 11. Overview of optical methods. Optical spectral instruments. Applications in the analysis of environmental components; Advantages, disadvantages. 12. Emission atomic spectral analysis. Flame photometry. Atomic absorption spectrometry. UV / Vis spectrometry. Applications in the analysis of environmental components; Advantages, disadvantages. 13. IR spectrometry. Raman spectra; X-ray fluorescence spectrometry. Applications in the analysis of environmental components; Advantages, disadvantages. 14. New trends in instrumental methods with application in the analysis of environmental components

Conditions for subject completion

Full-time form (validity from: 2022/2023 Winter semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of points
Credit and Examination Credit and Examination 100 (100) 51
        Credit Credit 33 (33) 17
                Laboratory protocols Laboratory work 20  11
                Credit test Written test 10  6
                Activity Other task type 3  0
        Examination Examination 67  25
Mandatory attendence parzicipation: 28 + 42 h/s

Show history

Occurrence in study plans

Academic yearProgrammeField of studySpec.ZaměřeníFormStudy language Tut. centreYearWSType of duty
2022/2023 (B0724HGF011) Environmental Protection within Industry K Czech Ostrava 3 Compulsory study plan
2022/2023 (B0724HGF011) Environmental Protection within Industry P Czech Ostrava 3 Compulsory study plan

Occurrence in special blocks

Block nameAcademic yearForm of studyStudy language YearWSType of blockBlock owner