546-0396/01 – Instrumental Methods of Analysis II (IMA II)

Gurantor departmentDepartment of Environmental EngineeringCredits8
Subject guarantordoc. Mgr. Eva Pertile, Ph.D.Subject version guarantordoc. Mgr. Eva Pertile, Ph.D.
Study levelundergraduate or graduateRequirementCompulsory
Year2Semestersummer
Study languageCzech
Year of introduction2006/2007Year of cancellation
Intended for the facultiesHGFIntended for study typesBachelor
Instruction secured by
LoginNameTuitorTeacher giving lectures
PER34 doc. Mgr. Eva Pertile, Ph.D.
Extent of instruction for forms of study
Form of studyWay of compl.Extent
Full-time Credit and Examination 2+4
Combined Credit and Examination 6+12

Subject aims expressed by acquired skills and competences

Knowledge acquired after the completion of the course: Acquiring basic knowledge of instrumental analytical methods and enhancing students' readiness to solve analytic problems by selected instrumental methods.Skills demonstrated at the end of the course: The student will gain the competence to work in an analytical laboratory with basic instrumental equipment.

Teaching methods

Lectures
Experimental work in labs
Terrain work
Other activities

Summary

The course is focused on broadening and deepening the knowledge of modern instrumental laboratory techniques, including gaining practical skills. The aim of the course is to provide students with a solid and sufficiently broad theoretical and methodological basis for methods of instrumental analysis, both inorganic and organic. The main focus of the lessons is the interpretation of the theoretical foundations of instrumental methods of analysis. Practical exercises emphasize students' independent approach to solving analytical problems of selected instrumental methods.

Compulsory literature:

PERTILE, E. Instrumental Methods of Analysis. Ostrava: Vysoká škola báňská - Technická univerzita Ostrava, 2017. ISBN 978-80-248-4124-3. SIVASANKAR, B. Instrumental methods of analysis. New Delhi: Oxford University Press, 2012. ISBN 9780198073918. BRICKER, B., ed. Experiments in analytical chemistry. London: Auris Reference, c2012. ISBN 978-1-78154-179-1. CHANG R.: Chemistry. 10th Edition. McGraw-Hill: New York, 2010. 1170 p. Available from: https://archive.org/details/Chemistry_10th_Edition_Raymond_Chang.4-3.

Recommended literature:

LONG, J. H. A textbook of elementary analytical chemistry: qualitative and volumetric. Lexington, KY: [CreateSpace Independent Publishing Platform], 2014. ISBN 978-1-4927-1822-2. TISSUE, B. M. Basics of analytical chemistry and chemical equilibria. Hoboken: Wiley, c2013. ISBN 978-0-470-59208-3. CAROLI, S. and G. ZÁRAY, ed. Analytical techniques for clinical chemistry: methods and applications. Hoboken: Wiley, c2012. ISBN 978-0-470-44527-3. GUARDIA, M. de la a S. GARRIGUES MATEO, ed. Handbook of green analytical chemistry. Chichester: Wiley, 2012. ISBN 978-0-470-97201-4.

Way of continuous check of knowledge in the course of semester

Student knowledge is verified in written form, emphasis is given to understanding the subject and applying theoretical knowledge to solving practical problems. The evaluation also includes collective evaluation and self-assessment. An active assessment of the students is also included in the class.

E-learning

Další požadavky na studenta

Active participation in the lectures and the seminars, demonstration of successful processing subtasks, entered continuously in the semester.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

1. Definition of issues. Basic concepts. Information retrieval processes. Analytical methods absolute and comparative. Calibration methods. Developmental trends in instrumental methods of environmental samples analysis. 2. Evaluation of the results of the analysis and the way of their expression with a focus on environmental analysis. Statistical evaluation of analytical results. Reference material, round test. Fundamentals of chemometric approaches and methods. 3. Testing the metrological properties of the results. Activity design resulting from the data obtained. 4. Electroanalytical methods: methods based on potential measurement (equilibrium potentiometry, potentiometric titration). Principles of individual methods; instrumentation; applications for environmental component analysis; Advantages, disadvantages. 5. Electroanalytical methods: current measurement methods. Voltammetry and polarography: Principles of individual methods; instrumentation; applications for environmental component analysis; Advantages, disadvantages. 6. Electrogravimetry and coulometry: a constant current and a constant potential. Conductometry. Principles of individual methods; instrumentation; applications for environmental component analysis; Advantages, disadvantages. 7. Optical analytical methods: theoretical basics. optical spectral devices. Methods without energy-to-radiation exchange (refractometry, polarimetry, nephelometry); Refractometry, Principles of individual methods; instrumentation; applications for environmental component analysis; Advantages, disadvantages. 8. Emission Atomic Spectral Analysis. Flame photometry. Atomic absorption spectrometry; UV / Vis spectrometry, Luminescence analysis. Fundamentals of theory, instrumentation, qualitative and quantitative aspects. Automatic analyzers with optical detection: FIA, CFA. Principles of individual methods; instrumentation; applications for environmental component analysis; Advantages, disadvantages. 9. Luminescence analysis. Infrared spectrometry. Raman spectra; X-ray fluorescence spectrometry. Radiochemical methods. Principles of individual methods, instrumentation, applications in environmental component analysis; Advantages, disadvantages. 10. Separation and concentration steps: theory. Separation methods: separation according to principle and according to experimental arrangement, efficiency of the separation process. Extraction. Instrumentation; applications for environmental component analysis; Advantages, disadvantages. 11. Membrane Separation. Mass spectrometry. Principles of individual methods; instrumentation; applications for environmental component analysis; Advantages, disadvantages. 12. Chromatographic methods. Planar Chromatography: Sorbent Thin Layer Chromatography, Fundamentals of Theory, Instrumentation, Qualitative and Quantitative Aspects, Applications. 13. Column chromatography: GC + HPLC. New Trends: UHPLC, GC / MS, HPLC / MS. Principles of individual methods; instrumentation; applications for environmental component analysis; Advantages, disadvantages. 14. Electromigration methods: theory, zonal and capillary electrophoresis, carrier electrophoresis and isotachophoresis. Principles of individual methods; instrumentation; applications for environmental component analysis; Advantages, disadvantages.

Conditions for subject completion

Combined form (validity from: 2011/2012 Summer semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of points
Exercises evaluation and Examination Credit and Examination 100 (100) 51
        Exercises evaluation Credit 30  15
        Examination Examination 70 (70) 36
                Written examination Written examination 33  18
                Oral Oral examination 37  18
Mandatory attendence parzicipation: Compulsory participation in exercises.

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Occurrence in study plans

Academic yearProgrammeField of studySpec.FormStudy language Tut. centreYearWSType of duty
2019/2020 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal P Czech Ostrava 2 Compulsory study plan
2019/2020 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Ostrava 2 Compulsory study plan
2019/2020 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Most 2 Compulsory study plan
2018/2019 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal P Czech Ostrava 2 Compulsory study plan
2018/2019 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Ostrava 2 Compulsory study plan
2018/2019 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Most 2 Compulsory study plan
2017/2018 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal P Czech Ostrava 2 Compulsory study plan
2017/2018 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Ostrava 2 Compulsory study plan
2017/2018 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Most 2 Compulsory study plan
2016/2017 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal P Czech Ostrava 2 Compulsory study plan
2016/2017 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Ostrava 2 Compulsory study plan
2016/2017 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Most 2 Compulsory study plan
2015/2016 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Ostrava 2 Compulsory study plan
2015/2016 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Most 2 Compulsory study plan
2015/2016 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal P Czech Ostrava 2 Compulsory study plan
2014/2015 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Ostrava 3 Compulsory study plan
2014/2015 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Most 3 Compulsory study plan
2013/2014 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Ostrava 3 Compulsory study plan
2013/2014 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Most 3 Compulsory study plan
2012/2013 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Ostrava 3 Compulsory study plan
2012/2013 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Most 3 Compulsory study plan
2011/2012 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Ostrava 3 Compulsory study plan
2011/2012 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Most 3 Compulsory study plan
2010/2011 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Ostrava 3 Compulsory study plan
2010/2011 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Most 3 Compulsory study plan
2009/2010 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Ostrava 3 Compulsory study plan
2009/2010 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Most 3 Compulsory study plan
2008/2009 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Ostrava 3 Compulsory study plan
2008/2009 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Most 3 Compulsory study plan
2007/2008 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Ostrava 3 Compulsory study plan
2007/2008 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Most 3 Compulsory study plan
2006/2007 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Ostrava 3 Compulsory study plan
2006/2007 (B2102) Mineral Raw Materials (3904R022) Waste Treatment and Disposal K Czech Most 3 Compulsory study plan

Occurrence in special blocks

Block nameAcademic yearForm of studyStudy language YearWSType of blockBlock owner
O - ECTS FMG - Bc. 2014/2015 Full-time Czech Optional 501 - Study Office stu. block
O - ECTS FMG - Bc. 2013/2014 Full-time Czech Optional 501 - Study Office stu. block
O - ECTS FMG - Bc. 2012/2013 Full-time Czech Optional 501 - Study Office stu. block