546-0940/02 – Instrumental Methods of Chemical Analysis (IMCH)

Gurantor departmentDepartment of Environmental EngineeringCredits10
Subject guarantordoc. Mgr. Eva Pertile, Ph.D.Subject version guarantordoc. Mgr. Eva Pertile, Ph.D.
Study levelpostgraduateRequirementChoice-compulsory
YearSemesterwinter + summer
Study languageCzech
Year of introduction1999/2000Year of cancellation
Intended for the facultiesHGFIntended for study typesDoctoral
Instruction secured by
LoginNameTuitorTeacher giving lectures
PER34 doc. Mgr. Eva Pertile, Ph.D.
Extent of instruction for forms of study
Form of studyWay of compl.Extent
Full-time Examination 20+0
Part-time Examination 20+0

Subject aims expressed by acquired skills and competences

The aim of the course is to expand theoretical knowledge and practical use of selected instrumental methods of chemical analysis of minerals, products of treatment and processing of environmental material. KNOWLEDGE PROVEN AFTER COMPLETING THE COURSE: Gaining an extension of basic knowledge not only about sampling in connection with its contribution to the overall uncertainty of the analysis but also from modern advanced instrumental methods of chemical analysis. They will be able to understand the use of analytical reactions in analysis; choose the right way of processing samples; characterize parameters important for instrumental methods; compare the possibilities of classical, electrochemical, spectrometric and separation methods; get an idea of the practical application of the methods. This will deepen their readiness for the independent solution of analytical problems by selected instrumental methods in solving their dissertation and subsequently in common analytical practice. SKILLS DEMONSTRATED AFTER COMPLETION OF THE COURSE: Acquisition of competence to work in an analytical laboratory, the ability to develop basic methods of analysis, presentation and evaluation of results, mastering the correct principles of work in the laboratory. They will be able to creatively choose the optimal method for solving specific analytical problems of analytical practice.

Teaching methods

Individual consultations

Summary

The course is focused on modern advanced analytical techniques, which the student may encounter in solving his dissertation and which are commonly used in control and development analytical laboratories. The aim is to expand and supplement the basic knowledge of instrumental methods of chemical analysis of mineral resources, products of treatment and processing of environmental materials. Emphasis is placed on understanding the principles, technical equipment and use of electrochemical, separation and optical methods.

Compulsory literature:

KENKEL J.: Analytical chemistry for technicians. 4th Edition, CRC Press, Boca Raton, 2013, 1-537. MILLER James, Jane C MILLER. Statistics and Chemometrics for Analytical Chemistry. Pearson Education Limited, 2018. ISBN: 1292186712. PERTILE, E. Instrumental Methods of Analysis. Ostrava: Vysoká škola báňská - Technická univerzita Ostrava, 2017. ISBN 978-80-248-4124-3. HARVEY T. D. Analytical Chemistry 2.1. Electronic Versions. 2016 http://dpuadweb.depauw.edu/harvey_web/eTextProject/AC2.1Files/AnalChem2.1.pdf.

Recommended literature:

FIELD L. D., STERNHELL S., KALMAN J. R. Organic Structures from Spectra. New York, United States: John Wiley & Sons Inc. 2013. ISBN 978-1-118-32549-0. PRETSCH E., BÜHLMANN P., BADERTSCHER M. Structure Determination of Organic Compounds : Tables of Spectral Data. Berlin, Germany: Springer-Verlag Berlin and Heidelberg GmbH & Co. KG. 2009. ISBN13 9783540938095. WEINER E.R. Applications of aquatic chemistry: a practical guide. 3rd edition, CRC Press, Boca Raton, 2012, 1-618. Analytical chemistry: a modern approach to analytical science. 2nd ed. Editor J.-M MERMET, editor M. OTTO, editor M. VALCÁRCEL. Weinheim: Wiley-VCH, c2004. ISBN 3527305904.

Way of continuous check of knowledge in the course of semester

regular contact with the teacher at individual consultations oral exam

E-learning

Other requirements

regular contact with the teacher at individual consultations

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

Information retrieval processes. Automation of measurement and data collection, continuous measurement of chemical characteristics in treatment. Evaluation of analytical results and procedures, expression of chemical analysis results. Statistical processing of results. Proposal of activities resulting from the obtained data. GLP principles. Methods of control of technological processes (development of analytical methods, the superstructure of analytical chemistry with a focus on industrial processes). Development and standardization of analytical methods. Operating procedures for sampling; QA / QC system. Sample preparation before analysis. Absolute and comparative analytical methods. Rapid analytical methods - screening. Calibration methods. Portable devices for the analysis of materials in landfills and in the field, parameters for their selection and evaluation. Selected electroanalytical methods applied in the analysis of mineral resources, treatment products and processing of environmental material. Sample preparation, application. Separation methods applied in the analysis of mineral raw materials, products of treatment and processing of environmental material - theoretical foundations and practical possibilities. Optical methods applied in the analysis of mineral resources, products of treatment and processing of environmental material. Sample preparation, application. Scanning probe surface analysis (STM, AFM, SNOM); photon probe (PES, XPS, UPS, LAMMS, etc.); electron probe (EPXMA, SEM, combined AEM, AES, etc.), ion probe (RBS, ISS, SIMS, etc.); pole probe (FIM, etc.). New trends in instrumental methods with application in conditioning. Coupling techniques GC-MS, LC-MS, CE-MS, GC / LC-ICP-MS, speciation analysis, LC / GC-IR, LC-NMR.

Conditions for subject completion

Full-time form (validity from: 2013/2014 Winter semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of pointsMax. počet pokusů
Examination Examination   3
Mandatory attendence participation:

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Conditions for subject completion and attendance at the exercises within ISP:

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Occurrence in study plans

Academic yearProgrammeBranch/spec.Spec.ZaměřeníFormStudy language Tut. centreYearWSType of duty
2023/2024 (P2116) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Choice-compulsory study plan
2022/2023 (P2116) Mineral Raw Materials (2102V009) Processing K Czech Ostrava Choice-compulsory study plan
2022/2023 (P2116) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Choice-compulsory study plan
2021/2022 (P2116) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Choice-compulsory study plan
2021/2022 (P2102) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Choice-compulsory study plan
2021/2022 (P2102) Mineral Raw Materials (2102V009) Processing K Czech Ostrava Choice-compulsory study plan
2020/2021 (P2102) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Choice-compulsory study plan
2020/2021 (P2116) Mineral Raw Materials (2102V009) Processing K Czech Ostrava Choice-compulsory study plan
2020/2021 (P2116) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Choice-compulsory study plan
2020/2021 (P2102) Mineral Raw Materials (2102V009) Processing K Czech Ostrava Choice-compulsory study plan
2019/2020 (P2102) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Choice-compulsory study plan
2019/2020 (P2102) Mineral Raw Materials (2102V009) Processing K Czech Ostrava Choice-compulsory study plan
2019/2020 (P2116) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Choice-compulsory study plan
2019/2020 (P2116) Mineral Raw Materials (2102V009) Processing K Czech Ostrava Choice-compulsory study plan
2018/2019 (P2116) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Choice-compulsory study plan
2018/2019 (P2116) Mineral Raw Materials (2102V009) Processing K Czech Ostrava Choice-compulsory study plan
2018/2019 (P2102) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Choice-compulsory study plan
2018/2019 (P2102) Mineral Raw Materials (2102V009) Processing K Czech Ostrava Choice-compulsory study plan
2017/2018 (P2102) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Choice-compulsory study plan
2017/2018 (P2102) Mineral Raw Materials (2102V009) Processing K Czech Ostrava Choice-compulsory study plan
2017/2018 (P2116) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Choice-compulsory study plan
2017/2018 (P2116) Mineral Raw Materials (2102V009) Processing K Czech Ostrava Choice-compulsory study plan
2016/2017 (P2102) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Choice-compulsory study plan
2016/2017 (P2102) Mineral Raw Materials (2102V009) Processing K Czech Ostrava Choice-compulsory study plan
2015/2016 (P2102) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Choice-compulsory study plan
2015/2016 (P2102) Mineral Raw Materials (2102V009) Processing K Czech Ostrava Choice-compulsory study plan
2014/2015 (P2102) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Choice-compulsory study plan
2014/2015 (P2102) Mineral Raw Materials (2102V009) Processing K Czech Ostrava Choice-compulsory study plan
2013/2014 (P2102) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Choice-compulsory study plan
2013/2014 (P2102) Mineral Raw Materials (2102V009) Processing K Czech Ostrava Choice-compulsory study plan
2012/2013 (P2102) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Choice-compulsory study plan
2012/2013 (P2102) Mineral Raw Materials (2102V009) Processing K Czech Ostrava Choice-compulsory study plan
2011/2012 (P2102) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Choice-compulsory study plan
2011/2012 (P2102) Mineral Raw Materials (2102V009) Processing K Czech Ostrava Choice-compulsory study plan
2010/2011 (P2102) Mineral Raw Materials (2102V009) Processing P Czech Ostrava Optional study plan
2010/2011 (P3904) Engineering Ecology (3904V012) Environment Protection within Industry P Czech Ostrava Optional study plan
2010/2011 (P2102) Mineral Raw Materials (2102V009) Processing K Czech Ostrava Optional study plan

Occurrence in special blocks

Block nameAcademic yearForm of studyStudy language YearWSType of blockBlock owner

Assessment of instruction



2019/2020 Winter