546-0940/02 – Instrumental Methods of Chemical Analysis (IMCH)
| Gurantor department | Department of Environmental Engineering | Credits | 10 |
| Subject guarantor | doc. Mgr. Eva Pertile, Ph.D. | Subject version guarantor | doc. Mgr. Eva Pertile, Ph.D. |
| Study level | postgraduate | Requirement | Choice-compulsory |
| Year | | Semester | winter + summer |
| | Study language | Czech |
| Year of introduction | 1999/2000 | Year of cancellation | |
| Intended for the faculties | HGF | Intended for study types | Doctoral |
Subject aims expressed by acquired skills and competences
The aim of the course is to expand theoretical knowledge and practical use of selected instrumental methods of chemical analysis of minerals, products of treatment and processing of environmental material.
KNOWLEDGE PROVEN AFTER COMPLETING THE COURSE: Gaining an extension of basic knowledge not only about sampling in connection with its contribution to the overall uncertainty of the analysis but also from modern advanced instrumental methods of chemical analysis. They will be able to understand the use of analytical reactions in analysis; choose the right way of processing samples; characterize parameters important for instrumental methods; compare the possibilities of classical, electrochemical, spectrometric and separation methods; get an idea of the practical application of the methods. This will deepen their readiness for the independent solution of analytical problems by selected instrumental methods in solving their dissertation and subsequently in common analytical practice. SKILLS DEMONSTRATED AFTER COMPLETION OF THE COURSE: Acquisition of competence to work in an analytical laboratory, the ability to develop basic methods of analysis, presentation and evaluation of results, mastering the correct principles of work in the laboratory. They will be able to creatively choose the optimal method for solving specific analytical problems of analytical practice.
Teaching methods
Individual consultations
Summary
The course is focused on modern advanced analytical techniques, which the student may encounter in solving his dissertation and which are commonly used in control and development analytical laboratories. The aim is to expand and supplement the basic knowledge of instrumental methods of chemical analysis of mineral resources, products of treatment and processing of environmental materials. Emphasis is placed on understanding the principles, technical equipment and use of electrochemical, separation and optical methods.
Compulsory literature:
Recommended literature:
Additional study materials
Way of continuous check of knowledge in the course of semester
regular contact with the teacher at individual consultations oral exam
E-learning
Other requirements
regular contact with the teacher at individual consultations
Prerequisities
Subject has no prerequisities.
Co-requisities
Subject has no co-requisities.
Subject syllabus:
Information retrieval processes. Automation of measurement and data collection, continuous measurement of chemical characteristics in treatment.
Evaluation of analytical results and procedures, expression of chemical analysis results. Statistical processing of results. Proposal of activities resulting from the obtained data. GLP principles.
Methods of control of technological processes (development of analytical methods, the superstructure of analytical chemistry with a focus on industrial processes). Development and standardization of analytical methods.
Operating procedures for sampling; QA / QC system. Sample preparation before analysis.
Absolute and comparative analytical methods. Rapid analytical methods - screening. Calibration methods. Portable devices for the analysis of materials in landfills and in the field, parameters for their selection and evaluation.
Selected electroanalytical methods applied in the analysis of mineral resources, treatment products and processing of environmental material. Sample preparation, application.
Separation methods applied in the analysis of mineral raw materials, products of treatment and processing of environmental material - theoretical foundations and practical possibilities.
Optical methods applied in the analysis of mineral resources, products of treatment and processing of environmental material. Sample preparation, application.
Scanning probe surface analysis (STM, AFM, SNOM); photon probe (PES, XPS, UPS, LAMMS, etc.); electron probe (EPXMA, SEM, combined AEM, AES, etc.), ion probe (RBS, ISS, SIMS, etc.); pole probe (FIM, etc.).
New trends in instrumental methods with application in conditioning. Coupling techniques GC-MS, LC-MS, CE-MS, GC / LC-ICP-MS, speciation analysis, LC / GC-IR, LC-NMR.
Conditions for subject completion
Occurrence in study plans
Occurrence in special blocks
Assessment of instruction