615-0903/02 – Methods of Instrumental Analysis I (MIA1)

Gurantor departmentDepartment of Analytic Chemistry ProcessesCredits10
Subject guarantorprof. Ing. Petr Praus, Ph.D.Subject version guarantorprof. Ing. Petr Praus, Ph.D.
Study levelpostgraduateRequirementChoice-compulsory
YearSemesterwinter + summer
Study languageEnglish
Year of introduction2013/2014Year of cancellation2013/2014
Intended for the facultiesFMTIntended for study typesDoctoral
Instruction secured by
LoginNameTuitorTeacher giving lectures
PRA37 prof. Ing. Petr Praus, Ph.D.
Extent of instruction for forms of study
Form of studyWay of compl.Extent
Full-time Examination 0+0
Part-time Examination 0+0

Subject aims expressed by acquired skills and competences

The aim of the course is the interpretation of the theory and practical exercises selected instrumental methods. The course focuses on the methods with which the graduate is likely to encounter in their practice.

Teaching methods

Lectures
Seminars
Individual consultations

Summary

Compulsory literature:

PRAUS, P., PLACHÁ, D. Vybrané kapitoly z instrumentální analýzy. Studijní opora, Ostrava: VŠB-TUO, 2009. SOMMER, L. a kol. Základy analytické chemie I a II. Skriptum, Brno: VUTIUM, 2000. HOLBECHER, Z., CHURÁČEK, J. Analytická chemie. Praha: SNTL, 1987.

Recommended literature:

COLTHUP, N. B., DALY, L. H., WIBERLEY, S. E. Introduction to Infrared and Raman Spectrometry. Breinigsville: Academic Press, 2009. BOČEK, P., DEML, P., GEBAUER, P., DOLNÍK, V. Analytická izotachoforéza. Praha: Academia, 1987.

Way of continuous check of knowledge in the course of semester

E-learning

Other requirements

There are no additional requirements for students.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

Atomic spectral analysis: Properties of light, interaction of light with matter. Model of the atom, the formation and properties of atomic emission spectra. Methods atomization and excitation monochromators and detectors. Interaction of X-ray radiation with matter, the formation of X-ray spectra, X-ray source, sample preparation, dispersion X-ray radiation. Atomic absorption spectrum, radiation sources, methods of atomization, correct measurements, monochromators, detectors, mercury analyzers. Instrumentation and sample preparation applications. Molecular spectral analysis: Interaction of molecules and the electromagnetic radiation. The emergence of molecular (electron) spectra of vibration and rotation of molecules. Rayleigh and Raman scattering. Instrumentation and sample preparation applications. Electrochemical methods: The electrochemical potential of the second electrode conductivity of weak and strong electrolytes, conductivity measurement, polarographic curves, DS and AC methods, stripping voltammetry, instrumentation and sample preparation applications. Electrophoretic separation methods: Migration of ions in an electric field, electroosmotic flow, surface and capillary electrophoresis, capillary isotachophoresis. Instrumentation and sample preparation applications.

Conditions for subject completion

Part-time form (validity from: 2013/2014 Winter semester, validity until: 2013/2014 Summer semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of points
Examination Examination  
Mandatory attendence parzicipation:

Show history

Occurrence in study plans

Academic yearProgrammeField of studySpec.ZaměřeníFormStudy language Tut. centreYearWSType of duty
2013/2014 (P3909) Process engineering (3909V003) Process engineering P Czech Ostrava Choice-compulsory study plan
2013/2014 (P3909) Process engineering (3909V003) Process engineering K Czech Ostrava Choice-compulsory study plan

Occurrence in special blocks

Block nameAcademic yearForm of studyStudy language YearWSType of blockBlock owner