617-0973/01 – Analysis of Fuels (AP)

Gurantor departmentDepartment of ChemistryCredits10
Subject guarantordoc. Mgr. Lucie Bartoňová, Ph.D.Subject version guarantordoc. Mgr. Lucie Bartoňová, Ph.D.
Study levelpostgraduateRequirementChoice-compulsory type B
YearSemesterwinter + summer
Study languageCzech
Year of introduction2019/2020Year of cancellation
Intended for the facultiesFMTIntended for study typesDoctoral
Instruction secured by
LoginNameTuitorTeacher giving lectures
BAR57 doc. Mgr. Lucie Bartoňová, Ph.D.
Extent of instruction for forms of study
Form of studyWay of compl.Extent
Full-time Examination 20+0
Part-time Examination 20+0

Subject aims expressed by acquired skills and competences

Student will be able: -to distinguish individual types of solid, liquid and gaseous fuels, -to characterize representative sampling procedures prior to fuel analysis, -to describe the most common separation methods for the fractionation of carbohydrate samples, -to explain principles of classical methods of mineral, textural, mechanical, thermal-physical and petrographic analyses, -to characterize utilization of spectrographic methods in analysis of fuels, -to describe methods of determination of physical-chemical characteristics of liquid and gaseous fuels, -to compare utilization of instrumental methods of analysis of liquid and gaseous fuels.

Teaching methods

Lectures
Individual consultations

Summary

Students will be acquainted with methods of solid, liquid and gaseous fuels analysis including procedures of representative sampling, separation and sample preparation techniques prior to analysis itself. Attention will be paid to analysis of chemical, physical-chemical, textural and mechanical characteristics as well as modern instrumental methods of fuels analysis.

Compulsory literature:

GAUGLITZ, G. , VO-DINH, T. (Eds.) Handbook of Spectroscopy. Wienheim: Wiley-VCH Verlag, 2003, ISBN 3-527-29782-0. McMASTER, M. (Ed.) HPLC – a practical user´s guide. Hoboken: John Wiley & Sons, 2007, ISBN 13-978-0-471-75401-5. SPEIGHT, J. G. Handbook of Coal Analysis [online]. Hoboken: John Wiley & Sons, 2015, Print ISBN:9781118369241, Online ISBN:9781119037699, DOI:10.1002/9781119037699, 364 p. https://onlinelibrary.wiley.com/doi/book/10.1002/9781119037699. SPEIGHT, J. G. Handbook of Petroleum Product Analysis, 2nd Edition [online]. Hoboken: John Wiley & Sons, 2015, Print ISBN:9781118369265, Online ISBN:9781118986370, DOI:10.1002/9781118986370. https://onlinelibrary.wiley.com/doi/book/10.1002/978111898637 HUGGINS, F.E. Overview of analytical methods for inorganic constituents in coal. International Journal of Coal Geology 2002, roč. 50, s. 169-214. ISSN: 0166-5162.

Recommended literature:

MITRA, S. (Ed.) Sample Preparation Techniques in Analytical Chemistry. Hoboken: John Wiley & Sons, 2003. ISBN 0-471-32845-6. HSU, Chang S. Diesel Fuels Analysis. In: R.A. Meyers (Ed.): Encyclopedia of Analytical Chemistry, pp. 6613-6622. Chichester: John Wiley & Sons, 2006. Print ISBN: 9780471976707, Online ISBN: 9780470027318, DOI: 10.1002/9780470027318. https://onlinelibrary.wiley.com/doi/book/10.1002/9780470027318.

Way of continuous check of knowledge in the course of semester

Presentation of seminar paper and oral exam.

E-learning

Other requirements

Individual requirements are based on PhD thesis subject.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

Overall classification of solid, liquid and gaseous fuels and particularities of their analysis, methods of representative sampling, separation methods for fractionation of carbohydrate samples. Analysis of solid fuels: methods classification, sample preparation prior to analysis itself, determination of moisture, ash content, volatile matter, ultimate analysis (C, H, N, S, O), methods of inorganic constituents analysis (elemental composition, mineral phases analysis, speciation analysis), physical and textural coal properties (density, porosity, specific surface area etc.), thermal-physical characteristics, caking and mechanical properties, petrographic analysis and coal rank, coal extraction and analysis, utilization of spectrographic methods in solid fuels analysis, classification and assessment of solid fuels quality. Analysis of liquid and gaseous fuels: group analysis, methods of physical-chemical characteristics determination (boiling point, flash and fire point, pour point, melting and softening point, density, viscosity, calorific value, surface tension, mechanical, oxidation and thermal stabilities, etc.), water and ash content, determination of average molecular weight, acidity, octane rating, cetane number, iodine value, aniline point, refractive index, analytical utilization of chromatographic methods, spectrographic analysis – infrared spectroscopy, mass spectroscopy, nuclear magnetic resonance, UV-VIS spectroscopy, X-ray diffraction analysis, X-ray fluorescence analysis etc., classification and assessment of liquid and gaseous fuels quality.

Conditions for subject completion

Full-time form (validity from: 2019/2020 Winter semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of points
Examination Examination  
Mandatory attendence parzicipation:

Show history

Occurrence in study plans

Academic yearProgrammeField of studySpec.ZaměřeníFormStudy language Tut. centreYearWSType of duty
2020/2021 (P0713D070001) Thermal engineering and fuels in industry K Czech Ostrava Choice-compulsory type B study plan
2020/2021 (P0713D070001) Thermal engineering and fuels in industry P Czech Ostrava Choice-compulsory type B study plan
2019/2020 (P0713D070001) Thermal engineering and fuels in industry P Czech Ostrava Choice-compulsory type B study plan
2019/2020 (P0713D070001) Thermal engineering and fuels in industry K Czech Ostrava Choice-compulsory type B study plan

Occurrence in special blocks

Block nameAcademic yearForm of studyStudy language YearWSType of blockBlock owner