617-3016/01 – Identification of Substances (IL)

Gurantor departmentDepartment of ChemistryCredits5
Subject guarantordoc. Ing. Michal Ritz, Ph.D.Subject version guarantordoc. Ing. Michal Ritz, Ph.D.
Study levelundergraduate or graduateRequirementCompulsory
Year2Semesterwinter
Study languageCzech
Year of introduction2019/2020Year of cancellation
Intended for the facultiesFMTIntended for study typesFollow-up Master
Instruction secured by
LoginNameTuitorTeacher giving lectures
PAV57 Ing. Jiří Pavlovský, Ph.D.
RIT37 doc. Ing. Michal Ritz, Ph.D.
Extent of instruction for forms of study
Form of studyWay of compl.Extent
Full-time Credit and Examination 2+2

Subject aims expressed by acquired skills and competences

Objective of the course - aims of the course unit: To teach students the basis of evaluation of the results of selected methods (XRD, NMR, vibration spectroscopy, MS, ...) for identification of chemical compounds and substances. Acquired knowledge: theoretical and practical knowledge of the spectra of selected analytical methods for the identification of chemical compounds and substances. Acquired skills: ability to evaluate the spectra of selected analytical methods for the identification of chemical compounds and substances.

Teaching methods

Lectures
Tutorials
Other activities

Summary

Subject deals with structure of chemical compounds description from either theoretic (simulation and theoretic calculations) or practical (intensification of spectral and separation methods of instrumental structural analysis) point of view.

Compulsory literature:

FIELD, L. D., STERNHELL, S., and KALMAN, J.R. Organic Structures from Spectra, 4th Edition. Chichester: John Wiley & Sons Ltd, 2008. ISBN 978-0-470-31926-0.

Recommended literature:

COLOMBINI, M.P. and MODUGNO, F. Organic mass spectrometry in art and archeology. Chichester: Willey, 2009. ISBN: 978-0-470-51703-1. CLERC, T. Structural Analysis of Organic Compounds by Combined Application of Spectroscopic Methods (Studies in analytical chemistry). Elsevier Science Ltd, 1981. ISBN 13 9780444997487.

Way of continuous check of knowledge in the course of semester

Delivery of protocols in the required quality. Oral exam.

E-learning

Other requirements

Understandig of qualitative intepretation of spectra of selected methods.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

-Nuclear magnetic resonance: principle of the method, instrumentation, measurement techniques, NMR spectra and their interpretation Mass spectroscopy: method principle, instrumentation, measurement techniques, MS spectra and their interpretation -Rentgen diffraction analysis: interpretation of XRD records for identification of chemical compounds a substances -Vibration spectroscopy: Interpretation of vibrational spectra for identification of chemical compounds a substances -Nuclear Magnetic Resonance: Interpretation of NMR spectra for identification of chemical compounds a substances Mass Spectroscopy: The interpretation of mass spectra for identification of chemical compounds a substances -Luminiscent spectroscopy: interpretation of luminescence spectra for identification of chemical compounds a substances

Conditions for subject completion

Full-time form (validity from: 2019/2020 Winter semester, validity until: 2020/2021 Summer semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of pointsMax. počet pokusů
Credit and Examination Credit and Examination 100 (100) 51
        Credit Credit 45  20
        Examination Examination 55  6 3
Mandatory attendence participation: Points-scoring credit and exam.

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Conditions for subject completion and attendance at the exercises within ISP:

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Occurrence in study plans

Academic yearProgrammeBranch/spec.Spec.ZaměřeníFormStudy language Tut. centreYearWSType of duty
2021/2022 (N0712A130004) Chemical and environmental engineering (S03) Methods of Analysis for Chemical and Environmental Engineering AMI P Czech Ostrava 2 Compulsory study plan
2020/2021 (N0712A130004) Chemical and environmental engineering (S03) Methods of Analysis for Chemical and Environmental Engineering AMI P Czech Ostrava 2 Compulsory study plan
2019/2020 (N0712A130004) Chemical and environmental engineering (S03) Methods of Analysis for Chemical and Environmental Engineering AMI P Czech Ostrava 2 Compulsory study plan

Occurrence in special blocks

Block nameAcademic yearForm of studyStudy language YearWSType of blockBlock owner

Assessment of instruction



2021/2022 Winter