635-0079/01 – Properties of Ceramic Materials II (VKM II)
| Gurantor department | Department of Thermal Engineering | Credits | 5 |
| Subject guarantor | doc. Ing. Václava Tomková, CSc. | Subject version guarantor | doc. Ing. Václava Tomková, CSc. |
| Study level | undergraduate or graduate | Requirement | Compulsory |
| Year | 5 | Semester | winter |
| | Study language | Czech |
| Year of introduction | 1965/1966 | Year of cancellation | 2009/2010 |
| Intended for the faculties | FMT | Intended for study types | Master |
Subject aims expressed by acquired skills and competences
1 Student will be able to characterize the basic methods of chemical analysis of ceramic and raw materials.
2 Student will be able to characterize and apply the basic methods of phase analysis of ceramic and raw materials.
3 Student will be able to choose a strategy and methods of chemical and phase analysis of ceramic and raw materials.
Teaching methods
Lectures
Seminars
Individual consultations
Experimental work in labs
Summary
Relationship among chemical and phase composition and properties of ceramic
materials. The methods of chemical analysis of ceramic materials. Possibility
of phase composition identification of ceramic materials.
Compulsory literature:
1.KALOUS, V. Metody chemického výzkumu. Praha : SNTL, 1987. 430 s.
2.ŠESTÁK, J. Měření termofyzikálních vlastností pevných látek. Praha :
Academia, 1982. 345 s.
3.KLIKA, Z., PRAUS, P. Analytická chemie I. Ostrava : VŠB-TU, 2002. 172 s.
Recommended literature:
Way of continuous check of knowledge in the course of semester
Protokoly a laboratorní cvičení.
E-learning
Other requirements
Prerequisities
Subject has no prerequisities.
Co-requisities
Subject has no co-requisities.
Subject syllabus:
Lectures:
1 Gravimetric procedure in chemical analysis, principle.
2 Volumetric analysis - Neutralization, Chelatometry. The indicators in
volumetric analysis, examples.
3 Principle of spectral separation methods and chemical analysis. Absorption spectral
analysis, Lambert - Beer law. Colorimetry, photometry, spectrophotometry.
4 Emission spectral analysis. X-ray fluorescence analysis.
5 Overview of methods of phase analysis.
6 DTA, TG, dilatometry and thermo-mechanical analysis. Simultaneous thermal analysis
applications.
7 Principle of DSC calorimetry.
8 Calvets - Tian's equation in calorimetry applications. The basic methodology for
calorimetric measurements.
9 X-ray diffraction, Bragg equation, applications. X-ray, formation, monochromatization, utilization.
10 X-ray diffraction phase analysis - identification one substance. X-ray procedure phase
analysis of mixtures of minerals.
11 X-ray microanalysis, the principle use
12 Principles and applications of the TEM imaging.
13 Principles, and applications of SEM imaging (REM).
Seminars:
1 Preparation of solutions for chemical analysis. Expressing the composition of
standard solutions, determine the titre. Decomposition of samples for chemical
analysis, storage solution.
2 Determination of SiO2 + non decomposable share R2O3 determination, determination
of loss on drying and annealing.
3 Volumetric determination of CaO and MgO.
4 Photometric determination of Fe2O3.
5 DTA - evaluation of measurement applications. TG - analysis of data usage.
6 X-ray diffraction phase analysis..
Conditions for subject completion
Occurrence in study plans
Occurrence in special blocks
Assessment of instruction
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