635-0821/01 – Identification of Chemical and Phase Composition (IDCHF)

Gurantor departmentDepartment of Thermal EngineeringCredits6
Subject guarantordoc. Ing. Jozef Vlček, Ph.D.Subject version guarantordoc. Ing. Jozef Vlček, Ph.D.
Study levelundergraduate or graduateRequirementChoice-compulsory
Year2Semesterwinter
Study languageCzech
Year of introduction2004/2005Year of cancellation
Intended for the facultiesFMTIntended for study typesFollow-up Master
Instruction secured by
LoginNameTuitorTeacher giving lectures
TOP36 Ing. Michaela Topinková, Ph.D.
VLC37 doc. Ing. Jozef Vlček, Ph.D.
Extent of instruction for forms of study
Form of studyWay of compl.Extent
Full-time Credit and Examination 2+3
Combined Credit and Examination 16+0

Subject aims expressed by acquired skills and competences

1 Student will be able to characterize the basic methods of chemical analysis of ceramic and raw materials. 2 Student will be able to characterize and apply the basic methods of phase analysis of ceramic and raw materials. 3 Student will be able to choose a strategy and methods of chemical and phase analysis of ceramic and raw materials.

Teaching methods

Lectures
Seminars
Individual consultations
Experimental work in labs

Summary

Relationship among chemical and phase composition and properties of ceramic materials. The methods of chemical analysis of ceramic materials. Possibility of phase composition identification of ceramic materials.

Compulsory literature:

1.Kubaschewski O. et al. Metallurgical Thermochemistry. Pergamon Press, London 1974.

Recommended literature:

1.Barin, I., Knacke, O. Thermochemical properties of inorganic substance. Springer Verlag, Berlin, 1973.

Way of continuous check of knowledge in the course of semester

Two continuous assessment tests.

E-learning

in preparation

Další požadavky na studenta

There are no other requirements.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

Lectures: 1.Gravimetric procedure in chemical analysis, principle. 2.Volumetric analysis - Neutralization, Chelatometry. The indicators in volumetric analysis, examples. 3.Principle of spectral separation methods and chemical analysis. Absorption spectral analysis, Lambert - Beer law. Colorimetry, photometry, spectrophotometry. 4.Emission spectral analysis. X-ray fluorescence analysis. 5.Overview of methods of phase analysis. 6.DTA, TG, dilatometry and thermo-mechanical analysis. Simultaneous thermal analysis applications. 7.Principle of DSC calorimetry. 8.Calvets - Tian's equation in calorimetry applications. The basic methodology for calorimetric measurements. 9.X-ray diffraction, Bragg equation, applications. X-ray, formation, monochromatization, utilization. 10.X-ray diffraction phase analysis - identification one substance. X-ray procedure phase analysis of mixtures of minerals. 11.X-ray microanalysis, the principle use 12.Principles and applications of the TEM imaging. 13.Principles, and applications of SEM imaging (REM). Seminars: 1.Preparation of solutions for chemical analysis. Expressing the composition of standard solutions, determine the titre. Decomposition of samples for chemical analysis, storage solution. 2.Determination of SiO2 + non decomposable share R2O3 determination, determination of loss on drying and annealing. 3.Volumetric determination of CaO and MgO. 4.Photometric determination of Fe2O3. 5.DTA - evaluation of measurement applications. TG - analysis of data usage. 6.X-ray diffraction phase analysis..

Conditions for subject completion

Full-time form (validity from: 1960/1961 Summer semester, validity until: 2011/2012 Summer semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of points
Exercises evaluation and Examination Credit and Examination 100 (100) 51
        Exercises evaluation Credit 30 (30) 0
                Laboratory work Laboratory work 30  0
        Examination Examination 70 (70) 0
                Written examination Written examination 20  0
                Oral Oral examination 50  0
Mandatory attendence parzicipation:

Show history

Occurrence in study plans

Academic yearProgrammeField of studySpec.FormStudy language Tut. centreYearWSType of duty
2015/2016 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics P Czech Ostrava 2 Choice-compulsory study plan
2015/2016 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics K Czech Ostrava 2 Choice-compulsory study plan
2014/2015 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics K Czech Ostrava 2 Choice-compulsory study plan
2014/2015 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics P Czech Ostrava 2 Choice-compulsory study plan
2013/2014 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics P Czech Ostrava 2 Choice-compulsory study plan
2013/2014 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics K Czech Ostrava 2 Choice-compulsory study plan
2012/2013 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics P Czech Ostrava 2 Choice-compulsory study plan
2012/2013 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics K Czech Ostrava 2 Choice-compulsory study plan
2011/2012 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics P Czech Ostrava 2 Choice-compulsory study plan
2011/2012 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics K Czech Ostrava 2 Choice-compulsory study plan
2010/2011 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics K Czech Ostrava 2 Choice-compulsory study plan
2010/2011 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics P Czech Ostrava 2 Choice-compulsory study plan
2009/2010 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics P Czech Ostrava 2 Choice-compulsory study plan
2009/2010 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics K Czech Ostrava 2 Choice-compulsory study plan
2008/2009 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics K Czech Ostrava 2 Choice-compulsory study plan
2008/2009 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics P Czech Ostrava 2 Choice-compulsory study plan
2007/2008 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics K Czech Ostrava 2 Choice-compulsory study plan
2007/2008 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics P Czech Ostrava 2 Choice-compulsory study plan
2006/2007 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics K Czech Ostrava 2 Choice-compulsory study plan
2006/2007 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics P Czech Ostrava 2 Choice-compulsory study plan
2005/2006 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics K Czech Ostrava 2 Choice-compulsory study plan
2005/2006 (N2109) Metallurgical Engineering (2109T025) Thermal Engineering and Industrial Ceramics P Czech Ostrava 2 Choice-compulsory study plan

Occurrence in special blocks

Block nameAcademic yearForm of studyStudy language YearWSType of blockBlock owner