635-3013/02 – Identification of chemical and phase composition (IDCHF)

Gurantor departmentDepartment of Thermal EngineeringCredits5
Subject guarantordoc. Ing. Jozef Vlček, Ph.D.Subject version guarantordoc. Ing. Jozef Vlček, Ph.D.
Study levelundergraduate or graduate
Study languageEnglish
Year of introduction2014/2015Year of cancellation
Intended for the facultiesFMTIntended for study typesFollow-up Master
Instruction secured by
LoginNameTuitorTeacher giving lectures
TOP36 Ing. Michaela Topinková, Ph.D.
VLC37 doc. Ing. Jozef Vlček, Ph.D.
Extent of instruction for forms of study
Form of studyWay of compl.Extent
Full-time Credit and Examination 3+2
Combined Credit and Examination 16+0

Subject aims expressed by acquired skills and competences

- student will be able to choose the strategy and methods of chemical and phase analysis of ceramics raw materials and products - student will be able to evaluate suitability of application ceramics materials in according with theirs chemical and phase composition

Teaching methods

Lectures
Tutorials

Summary

The subject is focused to solving relations between chemical and phase composition of materials and theirs properties. There are presented fundamental methods of chemical and phase analysis of ceramics raw materials and products. The significant attention is paid to methods of determination phase composition of ceramics systems. Content of subject is x-ray diffraction, electron microscopy, methods of thermal analysis, calorimetry, infrared spectroscopy and nuclear magnetic resonance.

Compulsory literature:

[1] RAMACHANDRAN, V. S., BEAUDOIN, J. J. Handbook of Analytical Techniques in Concrete Science and Technology: Principles, Techniques, and Applications. New York: William Andrew Publishing, 2001. ISBN 0-8155-1437-9.

Recommended literature:

[1] MACKENZIE, K. J. D., SMITH, M. E. Multinuclear solid-state NMR of inorganic materials. Oxford: Pergamon, 2002. ISBN 0-08-043787-7.

Way of continuous check of knowledge in the course of semester

E-learning

Další požadavky na studenta

Making of semestral project and passing the progress tests.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

1. Gravimetric procedure in chemical analysis, principle. 2. Volumetric analysis - Neutralization, Chelatometry. The indicators in volumetric analysis, examples. 3. Principle of spectral separation methods and chemical analysis. Absorption spectral analysis, Lambert - Beer law. Colorimetry, photometry, spectrophotometry. 4. Emission spectral analysis. X-ray fluorescence analysis. 5. Overview of methods of phase analysis. 6. DTA, TG, dilatometry and thermo-mechanical analysis. Simultaneous thermal analysis applications. 7. Principle of DSC calorimetry. 8. Tian Calvets equation in calorimetry, applications. The basic methods for calorimetric measurements. 9. X-ray diffraction, Bragg equation, applications. X-ray, formation, monochromatization, utilization. 10. X-ray diffraction phase analysis - identification one substance. X-ray procedure phase analysis of mixtures of minerals. 11. X-ray microanalysis, the principle use. 12. Electron microscopy. Principles and applications of the TEM imaging. Principles and applications of SEM imaging (REM). 13. Infrared spectroscopy, principles and utilization in ceramic materials branch 14. Solid state MAS NMR spectroscopy. Spectrums evaluation of nuclide 29Si and 27Al for identification of products of hydration reactions.

Conditions for subject completion

Full-time form (validity from: 2014/2015 Winter semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of points
Credit and Examination Credit and Examination 100 (100) 51
        Credit Credit 25  15
        Examination Examination 75  36
Mandatory attendence parzicipation:

Show history
Combined form (validity from: 2014/2015 Winter semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of points
Credit and Examination Credit and Examination 100 (100) 51
        Credit Credit 25  15
        Examination Examination 75  36
Mandatory attendence parzicipation:

Show history

Occurrence in study plans

Academic yearProgrammeField of studySpec.FormStudy language Tut. centreYearWSType of duty
2017/2018 (N2109) Metallurgical Engineering (2109T039) Thermal Engineering and Ceramic Materials P English Ostrava 2 Choice-compulsory study plan
2016/2017 (N2109) Metallurgical Engineering (2109T039) Thermal Engineering and Ceramic Materials P English Ostrava 2 Choice-compulsory study plan

Occurrence in special blocks

Block nameAcademic yearForm of studyStudy language YearWSType of blockBlock owner
FMST 2019/2020 Full-time English Compulsory 601 - Study Office stu. block
FMMI 2018/2019 Full-time English Compulsory 601 - Study Office stu. block