651-2056/01 – Physico-chemical Methods of Study of Materials (CAT/FCMM)

Gurantor departmentDepartment of Chemistry and Physico-Chemical ProcessesCredits4
Subject guarantorMgr. Jan Filip, Ph.D.Subject version guarantorMgr. Jan Filip, Ph.D.
Study levelundergraduate or graduateRequirementCompulsory
Year2Semestersummer
Study languageCzech
Year of introduction2022/2023Year of cancellation
Intended for the facultiesFMTIntended for study typesBachelor
Instruction secured by
LoginNameTuitorTeacher giving lectures
FIL0159 Mgr. Jan Filip, Ph.D.
Extent of instruction for forms of study
Form of studyWay of compl.Extent
Full-time Examination 4+0

Subject aims expressed by acquired skills and competences

This lectures are focused on physico-chemical methods used in study of solid substances.

Teaching methods

Lectures

Summary

The lectures will be devoted to thermal methods, magnetometry, crystallographic methods, microscopic methods, Mössbauer spectroscopy, particle size distribution study and viscoelastic properties of matter.

Compulsory literature:

HODOROABA, Vasile Dan, Wolfgang E. S. UNGER a A. G. SHARD, eds. Characterization of nanoparticles: measurement processes for nanoparticles. Amsterdam: Elsevier, [2020]. Micro & nano technologies. ISBN 978-0-12-814183-0. KUMAR, Challa S.S.R., In-situ Characterization Techniques for Nanomaterials, 1st Edition, Springer, [2018]. ISBN 9783662563212. KAFLÉ, Bhim Prasad, Chemical Analysis and Material Characterization by Spectrophotometry, Elsevier, [2019]. ISBN 9780128148662. 9.

Recommended literature:

DE OLIVEIRA Osvlado Novais, Jr., M. FERREIRA, F. DE LIMA LEITE, A.L. DA RÓZ, eds. Nanocharacterization Techniques, William Andrew Publishing, [2017]. ISBN 9780323497787.

Way of continuous check of knowledge in the course of semester

Oral exam.

E-learning

Other requirements

Requirements will be specified in lectures.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

1. Optical microscopy (basic concepts, the principle of image formation, structural elements of optical microscopes, sample preparation, use). 2. Electron microscopy (basic concepts, principle of image formation, structural elements of electron microscopes, SEM, TEM, sample preparation, use of electron microscopy). 3. AFM - atomic force microscopy (division of SPM techniques, interaction of the tip with the surface, principle of AFM measurement, AFM structural elements, measuring modes, sample preparation, use of AFM). 4. Crystals, types of crystal structures, examples of stereochemistry of selected substances. 5. X-ray structural analysis - (origin of X-rays, interaction of X-rays with the sample, instrumentation, techniques of X-ray diffraction analysis, use of X-ray structural analysis for characterization of materials). 6. Methods of thermal analysis - (division of methods TA, TG and DTA analysis, measurement principle, instrumentation, sample preparation, use of TG and DTA analysis, detection of gaseous products using MS and IR). 7. Magnetometry (theoretical introduction, basic concepts and quantities; paramagnetism, diamagnetism and their chemical interpretations; measurement of magnetic susceptibility). 8. Mössbauer spectroscopy (Mössbauer phenomenon, experimental setup, parameters of the Mössbauer spectrum, Mösbauer spectroscopy in the external magnetic field, magnetism of nanomaterials, use of Mössbauer spectroscopy in the study of nanomaterials). 9. Study of surface energy of solids (definition of surface energy, equilibrium in a system with a curved phase interface, equilibrium in a three-phase system, wetting, contact angle, methods for determining surface energy). 10. Methods of studying particle size distribution (concept of particle size evaluation, division of methods. Screening analysis - principle, measurement realization; sedimentation methods; laser granulometry - principle, instrumentation, own measurement, evaluation of results; DLS - principle, instrumentation, own measurement, evaluation results, the use of microscopy to evaluate particle size). 11. Determination of specific surface area of ​​substances and pore size distribution (basic concepts, principle of method based on gas physisorption, instrumentation, adsorption isotherms, calculation of specific surface area, principle of evaluation of pore size distribution). 12. Viscoelastic properties of substances (elastic, viscous and viscoelastic materials, complex modulus of elasticity, internal damping).

Conditions for subject completion

Full-time form (validity from: 2022/2023 Winter semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of pointsMax. počet pokusů
Examination Examination 100  51 3
Mandatory attendence participation: Min. 80%.

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Conditions for subject completion and attendance at the exercises within ISP: Completion of all mandatory tasks within individually agreed deadlines.

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Occurrence in study plans

Academic yearProgrammeBranch/spec.Spec.ZaměřeníFormStudy language Tut. centreYearWSType of duty
2024/2025 (B0712P130001) Environmental technology P Czech Ostrava 2 Compulsory study plan
2023/2024 (B0712P130001) Environmental technology P Czech Ostrava 2 Compulsory study plan
2022/2023 (B0712P130001) Environmental technology P Czech Ostrava 2 Compulsory study plan

Occurrence in special blocks

Block nameAcademic yearForm of studyStudy language YearWSType of blockBlock owner

Assessment of instruction

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