651-2057/01 – Basics of Selected Experimental Chemical Methods (CAT/ZVEM)

Gurantor department	Department of Chemistry and Physico-Chemical Processes	Credits	5
Subject guarantor	prof. RNDr. Michal Otyepka, Ph.D.	Subject version guarantor	prof. RNDr. Michal Otyepka, Ph.D.
Study level	undergraduate or graduate	Requirement	Compulsory
Year	2	Semester	summer
		Study language	Czech
Year of introduction	2022/2023	Year of cancellation
Intended for the faculties	FMT	Intended for study types	Bachelor

Instruction secured by
Login	Name	Tuitor	Teacher giving lectures
OTY0005	prof. RNDr. Michal Otyepka, Ph.D.

Extent of instruction for forms of study
Form of study	Way of compl.	Extent
Full-time	Graded credit	0+5

Subject aims expressed by acquired skills and competences

The aim of the course is to get students acquainted with fundamental methodology and procedures used in laboratory practice.

Teaching methods

Experimental work in labs

Summary

Laboratory practise is focused on mastering fundamental methodology and procedures used in laboratory practice in the fields of synthesis and analysis of chemical substances. Students will get acquainted with fundamental chemical operations and procedures, which are routinely used in chemical syntheses and analyzes in chemical laboratories.

Compulsory literature:

McNair, H. M., Miller, J. M., Basic Gas Chromatography, Second Edition, Wiley-VCH, 2008, ISBN: 9780470439548

Recommended literature:

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Way of continuous check of knowledge in the course of semester

Credit.

E-learning

Other requirements

Requirements will be specified in laboratory exercises.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

• Adsorption (adsorption of oxalic acid on active charcoal) • Rectification (rektification of mixture of methanol/ethanol) • Thin layer chromatography – determination of vitamins of category B • Protein separation using discontinuous electrophoresis in a polyacrylamide gel (PAGE) • Determination of content of phosphoric acid in Coca-Cola • Determination of content of acetic acid in trade vinegar • Buffer capacity • Potentiometric determination of pK • Optical activity • Inversion of sucrose • Spectrophotometric determination of pK of indicator • Determination of molar absorption coeficient • Spectrophotometric determination in water analysis (PO43-, NH4+, NO2-, NO3-) • Volumetric determination in water analysis (CODMn, water hardness Ca2+, Mg2+, acid-base properties) • Capture and determination of nitrogen oxides in the atmosphere

Conditions for subject completion

Full-time form (validity from: 2022/2023 Winter semester)

Task name	Type of task	Max. number of points (act. for subtasks)	Min. number of points	Max. počet pokusů
Graded credit	Graded credit	100	51	3

Mandatory attendence participation: 100% participation in the laboratory exercises.

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Conditions for subject completion and attendance at the exercises within ISP: Completion of all mandatory tasks within individually agreed deadlines.

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Occurrence in study plans

Academic year	Programme	Form	Study language	Tut. centre	Year	Type of duty
2024/2025	(B0712P130001) Environmental technology	P	Czech	Ostrava	2	Compulsory	study plan
2023/2024	(B0712P130001) Environmental technology	P	Czech	Ostrava	2	Compulsory	study plan
2022/2023	(B0712P130001) Environmental technology	P	Czech	Ostrava	2	Compulsory	study plan

Occurrence in special blocks

Block name	Academic year	Form of study	Study language	Year	W	S	Type of block	Block owner

Assessment of instruction

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