653-3039/01 – Practicum in spectrometry (PS)

Gurantor department	Department of Materials Engineering and Recycling	Credits	2
Subject guarantor	doc. Ing. Jitka Malcharcziková, Ph.D.	Subject version guarantor	doc. Ing. Jitka Malcharcziková, Ph.D.
Study level	undergraduate or graduate	Requirement	Optional
Year		Semester	winter + summer
		Study language	Czech
Year of introduction	2022/2023	Year of cancellation
Intended for the faculties	FMT	Intended for study types	Follow-up Master

Instruction secured by
Login	Name	Tuitor	Teacher giving lectures
MAL37	doc. Ing. Jitka Malcharcziková, Ph.D.

Extent of instruction for forms of study
Form of study	Way of compl.	Extent
Full-time	Graded credit	2+0
Part-time	Graded credit	6+0

Subject aims expressed by acquired skills and competences

- student will be able to describe principles of spectrometry - student will be able to characterize OES and ED-XRF spectrometry methods - student will be able to prepare samples for analysis, perform measurements and evaluate the obtained data - student will be able to assess the suitability of using the OES and ED-XRF method

Teaching methods

Seminars
Tutorials

Summary

Předmět je zaměřen na problematiku nedestruktivní chemické analýzy kovových materiálů pomocí spektrometrie a na stanovení vybraných kovů v nekovových materiálech. Výuka bude probíhat formou prezentací, seminářů a laboratorních prací.

Compulsory literature:

JOOSTEN, H. G., et al. Atomic Emission Spectrometry: AES - Spark, Arc, Laser Excitation. De Gruyter, 2020, 315 s. ISBN 9783110527681. THIELE, G. Chemical Analysis of metal samples using Optical Emission Spectroscopy [online]. 2019. Dostupné z https://www.expertevents.com.au/wp-content/uploads/20191018-Glen-Thiele-Chemical-analysis-of-metal-samples-using-OES-copy-for-distribution.pdf.

Recommended literature:

GILMORE, Gordon. Practical gamma-ray spectrometry. 2nd ed. Chichester: Wiley, c2008, 387 s. ISBN 978-0-470-86196-7. NORDBERG, G. Handbook on the toxicology of metals. Burlington: Elsevier/Academic Press, 2007. ISBN 978-0-12-369413-3 b

Way of continuous check of knowledge in the course of semester

Progress tests, final test, reports of laboratory works.

E-learning

Other requirements

Complete all given tasks: Progress tests, final test, reports of laboratory works.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

Introduction to spectrometry, non-destructive chemical analysis Basic principles of optical emission spectrometry Basic principles of X-ray fluorescence spectrometry Preparation of samples for measurement Chemical analysis by OES method Chemical analysis by ED-XRF method Determination of chemical composition of selected metals and their alloys Determination of chemical composition of metallic waste Determination of selected elements in non-metallic materials (soils) Heavy metals in the environment Evaluation and processing of obtained results Assessment of the suitability of using the OES and ED-XRF method Advantages and disadvantages of using the OES and ED-XRF method for selected types of metallic materials

Conditions for subject completion

Full-time form (validity from: 2022/2023 Winter semester)

Task name	Type of task	Max. number of points (act. for subtasks)	Min. number of points	Max. počet pokusů
Graded credit	Graded credit	100	51	3

Mandatory attendence participation: Passing tests, submission of protocols from laboratory works.

Show history

Conditions for subject completion and attendance at the exercises within ISP: Completion of all compulsory tasks within individually agreed deadlines.

Show history

Occurrence in study plans

Academic year	Programme	Branch/spec.	Form	Study language	Tut. centre	Type of duty
2024/2025	(N0715A270002) Materials Engineering	(S02) Materials technologies and recycling	P	Czech	Ostrava	Optional	study plan
2024/2025	(N0715A270002) Materials Engineering	(S02) Materials technologies and recycling	K	Czech	Ostrava	Optional	study plan
2023/2024	(N0715A270002) Materials Engineering	(S02) Materials technologies and recycling	K	Czech	Ostrava	Optional	study plan
2023/2024	(N0715A270002) Materials Engineering	(S02) Materials technologies and recycling	P	Czech	Ostrava	Optional	study plan
2022/2023	(N0715A270002) Materials Engineering	(S02) Materials technologies and recycling	K	Czech	Ostrava	Optional	study plan
2022/2023	(N0715A270002) Materials Engineering	(S02) Materials technologies and recycling	P	Czech	Ostrava	Optional	study plan

Occurrence in special blocks

Block name	Academic year	Form of study	Study language	Year	W	S	Type of block	Block owner

Assessment of instruction

2022/2023 Summer