9360-0015/01 – Instrumental methods of analysis (IMA)

Gurantor departmentCNT - Nanotechnology CentreCredits6
Subject guarantorprof. Ing. Jana Seidlerová, CSc.Subject version guarantorprof. Ing. Jana Seidlerová, CSc.
Study levelundergraduate or graduateRequirementCompulsory
Year2Semesterwinter
Study languageCzech
Year of introduction2010/2011Year of cancellation2015/2016
Intended for the facultiesFMTIntended for study typesFollow-up Master
Instruction secured by
LoginNameTuitorTeacher giving lectures
JON0025 Ing. Jan Jonáš
MIR0007 Ing. Martina Mirošová
OTO30 RNDr. Hana Otoupalíková
PLA88 doc. Ing. Daniela Plachá, Ph.D.
SEI40 prof. Ing. Jana Seidlerová, CSc.
TOM90 Ing. Šárka Tomisová
Extent of instruction for forms of study
Form of studyWay of compl.Extent
Full-time Credit and Examination 2+3

Subject aims expressed by acquired skills and competences

The student will understand the principles of modern instrumental analytical methods used in the analysis of different materials. Ones will be able to design the analytical procedure to examine the results and understand the correlation between structure and chemical composition of materials.

Teaching methods

Lectures
Tutorials
Experimental work in labs

Summary

Předmět je zaměřen na moderní fyzikálně-chemické postupy analýzy v oblasti anorganické a organické analytické chemie. V úvodu budou posluchači seznámeni s postupy úpravy vzorků využívající např. mikrovlnné záření, extrakce apod. Budou podrobně vysvětleny fyzikálně chemické základy optických, elektrochemických i chromatografických metod. Z jednotlivých metod bude důraz kladen na ty metody, které se uplatňují při hodnocení chemického složení odpadů. V závěru budou zmíněné metody fázové a strukturní analýzy (termická analýza, rentgenová difrakce). Posluchači budou také seznámeni se základy chemometrie.

Compulsory literature:

Higson. S., P., J. Analytical Chemistry Oxford University Press, 2005. ISBN-10: 0-19-850289-3.

Recommended literature:

Hage D.: Analytical Chemistry and Quantitative Analysis, Pearson Education, 2010. ISBN: 9780321706805.

Way of continuous check of knowledge in the course of semester

E-learning

Další požadavky na studenta

For this subject other requirements for student are not determined.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

Chemical treatment of samples for inorganic and organic analysis (decomposition of the dry and wet, microwave digestion), separation techniques. - Introduction to instrumental methods of analysis. - Optical Methods of Chemical Analysis. Distribution. Physico-chemical principles. Atomic spectroscopy, molecular spectroscopy in the UV, IR and VIZ spectrum, mass and laser spectroscopy. Equipments. Applications. - Electrochemical Methods of chemical analysis. Physico-chemical principles. Basic methods. Equipments. Applications. - Basic methods of structural and phase analysis of inorganic materials (principle and application of thermal analysis, X-ray diffraction). Equipments. Applications. - Nuclear magnetic resonance spectroscopy (NMR), electron paramagnetic resonance (EPR), Raman spectroscopy, Mass spectroscopy (MS). Equipments. Applications. - Chromatographic separation methods. Liquid and ion chromatography, principle. Equipments. Applications. - Chromatographic separation methods. Gas chromatography, principles. Equipments. Applications.

Conditions for subject completion

Full-time form (validity from: 2010/2011 Winter semester, validity until: 2015/2016 Summer semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of points
Exercises evaluation and Examination Credit and Examination 100 (100) 51
        Exercises evaluation Credit 45 (45) 25
                Záznam laboratorních úloh Laboratory work 30  20
                Písemná prověrka znalostí Written test 15  5
        Examination Examination 55 (55) 15
                Písemná zkouška Written test 25  10
                Ústní prověrka znalostí Oral examination 30  15
Mandatory attendence parzicipation:

Show history

Occurrence in study plans

Academic yearProgrammeField of studySpec.FormStudy language Tut. centreYearWSType of duty
2015/2016 (N3923) Materials Engineering (3911T033) Material Recycling P Czech Ostrava 2 Compulsory study plan
2014/2015 (N3923) Materials Engineering (3911T033) Material Recycling P Czech Ostrava 2 Compulsory study plan
2013/2014 (N3923) Materials Engineering (3911T033) Material Recycling P Czech Ostrava 2 Compulsory study plan
2012/2013 (N3923) Materials Engineering (3911T033) Material Recycling P Czech Ostrava 2 Compulsory study plan
2011/2012 (N3923) Materials Engineering (3911T033) Material Recycling P Czech Ostrava 2 Compulsory study plan
2010/2011 (N3923) Materials Engineering (3911T033) Material Recycling P Czech Ostrava 2 Compulsory study plan

Occurrence in special blocks

Block nameAcademic yearForm of studyStudy language YearWSType of blockBlock owner