9360-0015/01 – Instrumental methods of analysis (IMA)
Gurantor department | CNT - Nanotechnology Centre | Credits | 6 |
Subject guarantor | prof. Ing. Jana Seidlerová, CSc. | Subject version guarantor | prof. Ing. Jana Seidlerová, CSc. |
Study level | undergraduate or graduate | Requirement | Compulsory |
Year | 2 | Semester | winter |
| | Study language | Czech |
Year of introduction | 2010/2011 | Year of cancellation | 2015/2016 |
Intended for the faculties | FMT | Intended for study types | Follow-up Master |
Subject aims expressed by acquired skills and competences
The student will understand the principles of modern instrumental analytical methods used in the analysis of different materials. Ones will be able to design the analytical procedure to examine the results and understand the correlation between structure and chemical composition of materials.
Teaching methods
Lectures
Tutorials
Experimental work in labs
Summary
Předmět je zaměřen na moderní fyzikálně-chemické postupy analýzy v oblasti anorganické a organické analytické chemie. V úvodu budou posluchači seznámeni s postupy úpravy vzorků využívající např. mikrovlnné záření, extrakce apod. Budou podrobně vysvětleny fyzikálně chemické základy optických, elektrochemických i chromatografických metod. Z jednotlivých metod bude důraz kladen na ty metody, které se uplatňují při hodnocení chemického složení odpadů. V závěru budou zmíněné metody fázové a strukturní analýzy (termická analýza, rentgenová difrakce). Posluchači budou také seznámeni se základy chemometrie.
Compulsory literature:
Higson. S., P., J. Analytical Chemistry Oxford University Press, 2005. ISBN-10: 0-19-850289-3.
Recommended literature:
Way of continuous check of knowledge in the course of semester
E-learning
Other requirements
For this subject other requirements for student are not determined.
Prerequisities
Subject has no prerequisities.
Co-requisities
Subject has no co-requisities.
Subject syllabus:
Chemical treatment of samples for inorganic and organic analysis (decomposition of the dry and wet, microwave digestion), separation techniques.
- Introduction to instrumental methods of analysis.
- Optical Methods of Chemical Analysis. Distribution. Physico-chemical principles. Atomic spectroscopy, molecular spectroscopy in the UV, IR and VIZ spectrum, mass and laser spectroscopy. Equipments. Applications.
- Electrochemical Methods of chemical analysis. Physico-chemical principles. Basic methods. Equipments. Applications.
- Basic methods of structural and phase analysis of inorganic materials (principle and application of thermal analysis, X-ray diffraction). Equipments. Applications.
- Nuclear magnetic resonance spectroscopy (NMR), electron paramagnetic resonance (EPR), Raman spectroscopy, Mass spectroscopy (MS). Equipments. Applications.
- Chromatographic separation methods. Liquid and ion chromatography, principle. Equipments. Applications.
- Chromatographic separation methods. Gas chromatography, principles. Equipments. Applications.
Conditions for subject completion
Occurrence in study plans
Occurrence in special blocks
Assessment of instruction
Předmět neobsahuje žádné hodnocení.