9360-0122/03 – Analytical Chemistry (CH-AN)

Gurantor departmentCNT - Nanotechnology CentreCredits3
Subject guarantordoc. Ing. Vladimír Tomášek, CSc.Subject version guarantordoc. Ing. Vladimír Tomášek, CSc.
Study levelundergraduate or graduateRequirementCompulsory
Year2Semestersummer
Study languageCzech
Year of introduction2019/2020Year of cancellation
Intended for the facultiesFMTIntended for study typesBachelor
Instruction secured by
LoginNameTuitorTeacher giving lectures
NEU057 Ing. Lucie Chlebíková, Ph.D.
OTO30 RNDr. Hana Otoupalíková
MIK39 Ing. Barbora Thomasová, Ph.D.
TOM24 doc. Ing. Vladimír Tomášek, CSc.
Extent of instruction for forms of study
Form of studyWay of compl.Extent
Full-time Examination 3+0

Subject aims expressed by acquired skills and competences

The goal is to acquire a view of basic methods of chemical analysis.

Teaching methods

Lectures

Summary

The subject give a view of methods of chemical analysis of materials. Attention will be particularly devoted, besides the common fundamentals of analytical chemistry and basic methods, on instrumental methods. Students will be acquainted with the basics of spectroscopic, electrochemical and separation methods. Attention will be devoted on applications for chemical composition analysis of materials.

Compulsory literature:

KENKEL, John. Analytical Chemistry for Technicians. Boca Raton: CRC Press, 2002. ISBN 978-1-4398-8105-7. MERMET, Jean-Michel, OTTO, M., VALCÁRCEL, M. Analytical chemistry, a modern approach to analytical science. Wiley - VCH, 2004. ISBN 3-527-30590-4

Recommended literature:

KELLNER, R., MERMET, M., OTTO, M. and WIDMER, H. M. Analytical Chemistry. Weinheim: Wiley-VCH, 1998. ISBN 3-527-28881-3

Way of continuous check of knowledge in the course of semester

Written and oral.

E-learning

Other requirements

For this subject other requirements for student are not determined.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

1. Introduction, sampling, sample preparation. 2. Gravimetric analysis. Required laboratory equipment, overview of gravimetric methods, application. 3. Volumetric analysis. Required laboratory equipment, overview of volumetric methods, application. 4. Introduction to electrochemical methods. Conductometry, potentiometry, theoretical foundations. Using for direct measurement and for determination of end of titration. 5. Voltammetry, principle. Polarography, voltammetry on solid electrodes. Instrumentation, applications. 6. Electrogravimetry and coulometry, principle. Instrumentation, applications. 7. Introduction to separation methods, theoretical foundations. Extraction, distillation, membrane separation. 8. Introduction to spectral analysis, theoretical foundations. Overview of spectral methods. 9. X-Ray spectral analysis, theoretical foundations, methods of excitation of X-rays. X-Ray fluorescence spectrometry (XRF), construction of spectrometers, examples of use. 10. Atomic emission spectrometry (AES), principle. Spark and arc excitation and excitation in glowing discharge. AES with inductively coupled plasma (ICP). Instrumentation, application. 11. Atomic absorption spectrometry, principle. Flame and electrothermal atomization, hydride generation, cold vapor mercury. Instrumentation, application. 12. Molecular absorption spectrometry, principle. Interaction of electromagnetic radiation with molecules. Spectrometry in visible and near ultraviolet range. Instrumentation, application. 13. Mass spectrometry. Radio-analytical methods. Electron spectrometry (Auger electrons, X-ray photoelectrons-XPS), secondary ion mass spectrometry. Instrumentation, application.

Conditions for subject completion

Full-time form (validity from: 2019/2020 Winter semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of points
Examination Examination 100  51
Mandatory attendence parzicipation: Attendance at lectures min. 80%.

Show history

Occurrence in study plans

Academic yearProgrammeField of studySpec.ZaměřeníFormStudy language Tut. centreYearWSType of duty
2021/2022 (B0719A270001) Nanotechnology P Czech Ostrava 2 Compulsory study plan
2020/2021 (B0719A270001) Nanotechnology P Czech Ostrava 2 Compulsory study plan
2019/2020 (B0719A270001) Nanotechnology P Czech Ostrava 2 Compulsory study plan

Occurrence in special blocks

Block nameAcademic yearForm of studyStudy language YearWSType of blockBlock owner