9360-0122/05 – Analytical Chemistry (CH-AN)
Gurantor department | CNT - Nanotechnology Centre | Credits | 3 |
Subject guarantor | doc. Ing. Vladimír Tomášek, CSc. | Subject version guarantor | doc. Ing. Vladimír Tomášek, CSc. |
Study level | undergraduate or graduate | Requirement | Compulsory |
Year | 2 | Semester | summer |
| | Study language | English |
Year of introduction | 2019/2020 | Year of cancellation | |
Intended for the faculties | FMT | Intended for study types | Bachelor |
Subject aims expressed by acquired skills and competences
The goal is to acquire a view of basic methods of chemical analysis.
Teaching methods
Lectures
Summary
The subject give a view of methods of chemical analysis of materials. Attention will be particularly devoted, besides the common fundamentals of analytical chemistry and basic methods, on instrumental methods. Students will be acquainted with the basics of spectroscopic, electrochemical and separation methods. Attention will be devoted on applications for chemical composition analysis of materials.
Compulsory literature:
Recommended literature:
Way of continuous check of knowledge in the course of semester
Written and oral.
E-learning
Other requirements
For this subject other requirements for student are not determined.
Prerequisities
Subject has no prerequisities.
Co-requisities
Subject has no co-requisities.
Subject syllabus:
1. Introduction, sampling, sample preparation.
2. Gravimetric analysis. Required laboratory equipment, overview of gravimetric methods, application.
3. Volumetric analysis. Required laboratory equipment, overview of volumetric methods, application.
4. Introduction to electrochemical methods. Conductometry, potentiometry, theoretical foundations. Using for direct measurement and for determination of end of titration.
5. Voltammetry, principle. Polarography, voltammetry on solid electrodes. Instrumentation, applications.
6. Electrogravimetry and coulometry, principle. Instrumentation, applications.
7. Introduction to separation methods, theoretical foundations. Extraction, distillation, membrane separation.
8. Introduction to spectral analysis, theoretical foundations. Overview of spectral methods.
9. X-Ray spectral analysis, theoretical foundations, methods of excitation of X-rays. X-Ray fluorescence spectrometry (XRF), construction of spectrometers, examples of use.
10. Atomic emission spectrometry (AES), principle. Spark and arc excitation and excitation in glowing discharge. AES with inductively coupled plasma (ICP).
Instrumentation, application.
11. Atomic absorption spectrometry, principle. Flame and electrothermal atomization, hydride generation, cold vapor mercury. Instrumentation, application.
12. Molecular absorption spectrometry, principle. Interaction of electromagnetic radiation with molecules. Spectrometry in visible and near ultraviolet range. Instrumentation, application.
13. Mass spectrometry. Radio-analytical methods. Electron spectrometry (Auger electrons, X-ray photoelectrons-XPS), secondary ion mass spectrometry. Instrumentation, application.
Conditions for subject completion
Occurrence in study plans
Occurrence in special blocks
Assessment of instruction
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