9360-0131/03 – Experimental methods and implements for nanotechnology I (EMAN)

Gurantor department	CNT - Nanotechnology Centre	Credits	5
Subject guarantor	doc. Mgr. Kateřina Mamulová Kutláková, Ph.D.	Subject version guarantor	doc. Mgr. Kateřina Mamulová Kutláková, Ph.D.
Study level	undergraduate or graduate	Requirement	Compulsory
Year	3	Semester	winter
		Study language	Czech
Year of introduction	2019/2020	Year of cancellation
Intended for the faculties	FMT, USP	Intended for study types	Bachelor

Instruction secured by
Login	Name	Tuitor	Teacher giving lectures
SEN05	Ing. Sylva Holešová, Ph.D.
STE17	Ing. Gabriela Kratošová, Ph.D.
MAM02	doc. Mgr. Kateřina Mamulová Kutláková, Ph.D.
PEI0007	Mgr. Pavlína Peikertová, Ph.D.
PLA88	prof. Ing. Daniela Plachá, Ph.D.
TOM24	doc. Ing. Vladimír Tomášek, CSc.
VAC121	Ing. Miroslav Vaculík, Ph.D.

Extent of instruction for forms of study
Form of study	Way of compl.	Extent
Full-time	Examination	3+0

Subject aims expressed by acquired skills and competences

The goal is to acquaint students with chemical methods and implements for structure a chemical composition study of nanomaterials.

Teaching methods

Lectures

Summary

The subject give fundamentals of transmition and scanning electron microscopy, scanning probe microscopy and X-ray diffraction methods. Students will be acquainted with application of the methods for structure, chemical and phase composition study of materials. Students will be also acquainted with some chosen methods of nanomaterials study (chromatography, electrophoresis, IR spectrometry, thermal analysis, NMR).

Compulsory literature:

BONNELL, D. editor. Scanning Probe Microscopy and Spectroscopy, Theory, Techniques and Applications. Wiley-VCH, 2001. YAO, Nan, WANG, Zhong Lin. Handbook of Microscopy for Nanotechnology. Springer US, 2005. ISBN 978-1-4020-8003-6.

Recommended literature:

WATT, I. M. The Principles and Practice of Electron Microscopy. Cambridge University Press. 1997. KENKEL, John. Analytical Chemistry for Technicians. Boca Raton: CRC Press, 2013. ISBN 978-1-4398-8105-7.

Way of continuous check of knowledge in the course of semester

Oral and written.

E-learning

Other requirements

For this subject other requirements for student are not determined.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

1. Introduction to chromatography, theoretical foundations. Overview of chromatographic methods, basic arrangement of chromatograph. 2. Gas chromatography. Basic apparatus construction, columns, detectors, evaluation of results, applications. 3. Liquid chromatography. Basic apparatus construction, columns, detectors, evaluation of results. 4. Electromigration methods, theoretical foundations. Electrophoresis, its use for analysis of organic compounds. 5. Introduction to electron microscopy, theoretical foundations, interaction of electron beam with sample. 6. Scanning and transmission electron microscopy. Construction of microscopes, their use in study of structure and chemical composition of materials. 7. Introduction to scanning probe microscopy, theoretical foundations. Interaction of mechanical probe with sample surface. 8.Atomic force microscopy (AFM) and scanning tunneling microscopy (STM). Apparatus construction, applications. 9. Introduction to diffraction methods, theoretical foundations, interaction of x-rays with crystal substances. 10. X-ray diffractometry, basic diffractometers construction. Use in study of crystal structure and phase composition of materials. 11. Thermal analysis, theoretical foundations. Thermogravimetry (TG), Difference thermal analysis (DTA), analytical use. 12. Introduction to infrared spectroscopy, theoretical foundations, interaction of infrared radiation with molecules. Construction of spectrometers, analytical use. 13. Raman spectroscopy, theoretical foundations. Apparatus construction, analytical use. 14.

Conditions for subject completion

Full-time form (validity from: 2019/2020 Winter semester)

Task name	Type of task	Max. number of points (act. for subtasks)	Min. number of points	Max. počet pokusů
Examination	Examination	100	51	3

Mandatory attendence participation: Attendance at lectures min. 80%. Passing the exam.

Show history

Conditions for subject completion and attendance at the exercises within ISP:

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Occurrence in study plans

Academic year	Programme	Zaměření	Form	Study language	Tut. centre	Year	Type of duty
2024/2025	(B0719A270001) Nanotechnology	EM	P	Czech	Ostrava	3	Compulsory	study plan
2023/2024	(B0719A270001) Nanotechnology	EM	P	Czech	Ostrava	3	Compulsory	study plan
2022/2023	(B0719A270001) Nanotechnology	EM	P	Czech	Ostrava	3	Compulsory	study plan
2021/2022	(B0719A270001) Nanotechnology	EM	P	Czech	Ostrava	3	Compulsory	study plan
2020/2021	(B0719A270001) Nanotechnology	EM	P	Czech	Ostrava	3	Compulsory	study plan
2019/2020	(B0719A270001) Nanotechnology	EM	P	Czech	Ostrava	3	Compulsory	study plan

Occurrence in special blocks

Block name	Academic year	Form of study	Study language	Year	W	S	Type of block	Block owner

Assessment of instruction

2021/2022 Winter