9360-0132/02 – Laboratory Practice from Experimetnal Methods of Nanomaterials Study I (LPEM)

Gurantor departmentCNT - Nanotechnology CentreCredits3
Subject guarantordoc. Ing. Vladimír Tomášek, CSc.Subject version guarantordoc. Ing. Vladimír Tomášek, CSc.
Study levelundergraduate or graduateRequirementCompulsory
Year3Semesterwinter
Study languageCzech
Year of introduction2012/2013Year of cancellation
Intended for the facultiesUSPIntended for study typesBachelor
Instruction secured by
LoginNameTuitorTeacher giving lectures
DRO105 Ing. Klára Drobíková, Ph.D.
STE17 Ing. Gabriela Kratošová, Ph.D.
LES05 Prof. Mgr. Jana Kukutschová, Ph.D.
MAM02 Mgr. Kateřina Mamulová Kutláková, Ph.D.
MAT27 doc. Ing. Vlastimil Matějka, Ph.D.
OTO30 RNDr. Hana Otoupalíková
PEI0007 Mgr. Pavlína Peikertová, Ph.D.
PLA88 doc. Ing. Daniela Plachá, Ph.D.
TOM24 doc. Ing. Vladimír Tomášek, CSc.
VAC121 Ing. Miroslav Vaculík, Ph.D.
Extent of instruction for forms of study
Form of studyWay of compl.Extent
Full-time Graded credit 0+4

Subject aims expressed by acquired skills and competences

Students will try different experimental techniques of nanomaterials study (SEM, EMA, AFM, XRD, chromatography, IR spectrometry, Raman spectrometry) in practice.

Teaching methods

Seminars
Experimental work in labs

Summary

Students will try different experimental techniques of nanomaterials study (SEM, EMA, AFM, XRD, chromatography, IR spectrometry, Raman spectrometry) in practice

Compulsory literature:

WATT, I,. M.: The principles and practice of electron microscopy. Cambridge University Press, 1997. JENKINS, R., SNYDER, R. L. Introduction to X-ray Powder Diffractometry. J.Wiley & Sons, 1996. BONNELL, D. editor: Scanning Probe Microscopy and Spectroscopy, Theory, Techniques and Applications. Wiley-VCH, 2001.

Recommended literature:

KENKEL, John. Analytical Chemistry for Technicians. Boca Raton: CRC Press, 2002. ISBN 978-1-4398-8105-7. YAO, N., WANG, Z., L. (editors). Handbook of Microscopy for Nanotechnology. Kluwer Academic Publishers, 2005.

Way of continuous check of knowledge in the course of semester

E-learning

Další požadavky na studenta

For this subject other requirements for student are not determined.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

1. Sample preparation for chromatography. Extraction, SPE, SPME, thermal dessorpion, headspace analysis. 2. Gas chromatography. Analysis of gas and BTEX, calibration, determination of basic parameters of separation. 3. Liquid chromatography. Analysis of anions. Calibration, determination of basic parameters of separation. Dectors on the basis of mass spectrometry. determination of structural compound formula on the basis of mass spectrum. 5. Identifying of asbestos using SEM + EMA method: a) analysis of morphology and chemical composition of asbestos and other fibrous materials b) analysis of an unknown sample of fibrous material, confirm or refute the presence of asbestos 6. Measuring of topography of semiconductor grid sample a) in contact mode b) in semi contact mode 7. Powder X-ray diffraction: a) measuring diffraction of powdered sample on the Si plate b) evaluation of diffraction record, identifying of compounds 8. Thermal analysis, evaluation of TG and DTA curves. 9. Infrared spectrometry 10 Raman spectrometry.

Conditions for subject completion

Full-time form (validity from: 2012/2013 Winter semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of points
Graded exercises evaluation Graded credit 100  51
Mandatory attendence parzicipation:

Show history

Occurrence in study plans

Academic yearProgrammeField of studySpec.FormStudy language Tut. centreYearWSType of duty
2019/2020 (B3942) Nanotechnology (3942R001) Nanotechnology P Czech Ostrava 3 Compulsory study plan
2018/2019 (B3942) Nanotechnology (3942R001) Nanotechnology P Czech Ostrava 3 Compulsory study plan
2017/2018 (B3942) Nanotechnology (3942R001) Nanotechnology P Czech Ostrava 3 Compulsory study plan
2016/2017 (B3942) Nanotechnology (3942R001) Nanotechnology P Czech Ostrava 3 Compulsory study plan
2015/2016 (B3942) Nanotechnology (3942R001) Nanotechnology P Czech Ostrava 3 Compulsory study plan
2014/2015 (B3942) Nanotechnology P Czech Ostrava 3 Compulsory study plan
2014/2015 (B3942) Nanotechnology (3942R001) Nanotechnology P Czech Ostrava 3 Compulsory study plan
2013/2014 (B3942) Nanotechnology (3942R001) Nanotechnology P Czech Ostrava 3 Compulsory study plan
2012/2013 (B3942) Nanotechnology (3942R001) Nanotechnology P Czech Ostrava 3 Compulsory study plan

Occurrence in special blocks

Block nameAcademic yearForm of studyStudy language YearWSType of blockBlock owner