9360-0142/04 – Nanomaterials characterization-laboratory practice (LCCN)

Gurantor departmentCNT - Nanotechnology CentreCredits3
Subject guarantordoc. Ing. Gražyna Simha Martynková, Ph.D.Subject version guarantordoc. Ing. Gražyna Simha Martynková, Ph.D.
Study levelundergraduate or graduateRequirementChoice-compulsory type B
Year2Semestersummer
Study languageCzech
Year of introduction2019/2020Year of cancellation
Intended for the facultiesUSP, FMTIntended for study typesFollow-up Master
Instruction secured by
LoginNameTuitorTeacher giving lectures
BAR31 Ing. Karla Čech Barabaszová, Ph.D. Paed.IGIP
SEN05 Ing. Sylva Holešová, Ph.D.
HUN019 Ing. Marianna Hundáková, Ph.D.
ZDR063 Ing. Jana Kupková, Ph.D.
PAZ065 Ing. Lenka Pazourková
SIM75 doc. Ing. Gražyna Simha Martynková, Ph.D.
CHM80 RNDr. Marta Valášková, DSc.
Extent of instruction for forms of study
Form of studyWay of compl.Extent
Full-time Graded credit 0+3

Subject aims expressed by acquired skills and competences

The knowledge in laboratory and analytical techniques for characterization of nanomaterials are main output of subject.

Teaching methods

Seminars
Tutorials
Experimental work in labs

Summary

The subject is focused on experimental methods of characterization of nanomaterials and is linked with subjects Nanomaterials based on natural materials and Methods of structural and phase analysis.

Compulsory literature:

YARIV S., CROSS H.: Organo-Clay Complexes and Interactions. New York, Basel, 2002, 688 p, ISBN 0-8247-0586-6. Fine Particles, Synthesis, Characterization and Mechanism of Growth. Edited by. T. Sugimoto. Marcel Dekker, New York, 2000. Nanostructure Science and Technology. Edited by Siengel, W., R., Hu, E., Roco, M., C. Kluwer Academic Publisher, London 1999. ISBN 0-7923-5854-6.

Recommended literature:

Vermiculite: structural properties and examples of the use; Valášková, Marta, Simha Martynkova, G.: Clay minerals in nature-their characterization, modification and application, InTech, 209-238,2012. Sneha Mohan Samuel Oluwatobi Oluwafemi Nandakumar Kalarikkal Sabu Thomas, eds.: Characterization of Nanomaterials, Woodhead Publishing, ISBN: 9780081019733.

Way of continuous check of knowledge in the course of semester

The student delivers on-going protocols with elaborated results of analyzes and conclusions.

E-learning

Other requirements

For this subject other requirements for student are not determined.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

1. Introduction to laboratory practice - introduction to the subject matter and conditions of its completion. Safety at work in the laboratory. . Preparation of different types of samples for chemical and structural analysis. 3. Mechanical processing (crushing, grinding, friction and homogenization). 4. Evaluation of particulate materials - size and distribution. 5. Morphological characterization of powders - microscopy. 6. Modification of layered materials and exfoliation-delamination. organophilization. 7. Embedding nanowires into the composite matrix. 8. Evaluation of nanoparticles in composites. 9.Infrared spectroscopy - structural analysis. 10. Raman spectroscopy structural analysis. 11. X-ray diffraction analysis phase and structural evaluation. 12.Termogravimetric analysis of temperature and materials conversion. 13. Quantitative and qualitative analysis of data comparison from different analytical methods. 14. Molecular modeling of structures and interaction.

Conditions for subject completion

Full-time form (validity from: 2019/2020 Winter semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of points
Graded credit Graded credit 100  51
Mandatory attendence parzicipation: classified credit based on point-evaluated protocols from individual exercises

Show history

Occurrence in study plans

Academic yearProgrammeField of studySpec.ZaměřeníFormStudy language Tut. centreYearWSType of duty
2021/2022 (N0719A270002) Nanotechnology P Czech Ostrava 2 Choice-compulsory type B study plan
2020/2021 (N0719A270002) Nanotechnology P Czech Ostrava 2 Choice-compulsory type B study plan
2019/2020 (N0719A270002) Nanotechnology P Czech Ostrava 2 Choice-compulsory type B study plan

Occurrence in special blocks

Block nameAcademic yearForm of studyStudy language YearWSType of blockBlock owner