9360-0142/05 – Nanomaterials characterization-laboratory practice (LCCN)

Gurantor department	CNT - Nanotechnology Centre	Credits	4
Subject guarantor	prof. Ing. Gražyna Simha Martynková, Ph.D.	Subject version guarantor	prof. Ing. Gražyna Simha Martynková, Ph.D.
Study level	undergraduate or graduate	Requirement	Compulsory
Year	2	Semester	summer
		Study language	English
Year of introduction	2019/2020	Year of cancellation
Intended for the faculties	FMT, USP	Intended for study types	Follow-up Master

Instruction secured by
Login	Name	Tuitor	Teacher giving lectures
BAR31	Ing. Karla Čech Barabaszová, Ph.D. Paed.IGIP
SEN05	Ing. Sylva Holešová, Ph.D.
HUN019	Ing. Marianna Hundáková, Ph.D.
PAZ065	Ing. Lenka Klecandová, Ph.D.
ZDR063	Ing. Jana Kupková, Ph.D.
SIM75	prof. Ing. Gražyna Simha Martynková, Ph.D.

Extent of instruction for forms of study
Form of study	Way of compl.	Extent
Full-time	Graded credit	0+3

Subject aims expressed by acquired skills and competences

The knowledge in laboratory and analytical techniques for characterization of nanomaterials are main output of subject.

Teaching methods

Seminars
Tutorials
Experimental work in labs

Summary

The subject is focused on experimental methods of characterization of nanomaterials and is linked with subjects Nanomaterials based on natural materials and Methods of structural and phase analysis.

Compulsory literature:

YARIV S., CROSS H.: Organo-Clay Complexes and Interactions. New York, Basel, 2002, 688 p, ISBN 0-8247-0586-6. Fine Particles, Synthesis, Characterization and Mechanism of Growth. Edited by. T. Sugimoto. Marcel Dekker, New York, 2000. Nanostructure Science and Technology. Edited by Siengel, W., R., Hu, E., Roco, M., C. Kluwer Academic Publisher, London 1999. ISBN 0-7923-5854-6.

Recommended literature:

Vermiculite: structural properties and examples of the use; Valášková, Marta, Simha Martynkova, G.: Clay minerals in nature-their characterization, modification and application, InTech, 209-238,2012. Sneha Mohan Samuel Oluwatobi Oluwafemi Nandakumar Kalarikkal Sabu Thomas, eds.: Characterization of Nanomaterials, Woodhead Publishing, ISBN: 9780081019733.

Additional study materials

Study supports in the EduDocs system

Way of continuous check of knowledge in the course of semester

The student delivers on-going protocols with elaborated results of analyzes and conclusions.

E-learning

Other requirements

For this subject other requirements for student are not determined.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

1. Introduction to laboratory practice - introduction to the subject matter and conditions of its completion. Safety at work in the laboratory. . Preparation of different types of samples for chemical and structural analysis. 3. Mechanical processing (crushing, grinding, friction and homogenization). 4. Evaluation of particulate materials - size and distribution. 5. Morphological characterization of powders - microscopy. 6. Modification of layered materials and exfoliation-delamination. organophilization. 7. Embedding nanowires into the composite matrix. 8. Evaluation of nanoparticles in composites. 9.Infrared spectroscopy - structural analysis. 10. Raman spectroscopy structural analysis. 11. X-ray diffraction analysis phase and structural evaluation. 12.Termogravimetric analysis of temperature and materials conversion. 13. Quantitative and qualitative analysis of data comparison from different analytical methods. 14. Molecular modeling of structures and interaction.

Conditions for subject completion

Full-time form (validity from: 2019/2020 Winter semester)

Task name	Type of task	Max. number of points (act. for subtasks)	Min. number of points	Max. počet pokusů
Graded credit	Graded credit	100	51	3

Mandatory attendence participation: For successful completion of the course it is obligatory to submit all evaluated protocols of laboratory exercises according to the prescribed list and to obtain at least more than half of the points for each protocol. Based on the sum of points will be awarded graded credit.

Show history

Conditions for subject completion and attendance at the exercises within ISP: Completion of the exam part tasks at least on minimum terms.

Show history

Occurrence in study plans

Academic year	Programme	Form	Study language	Tut. centre	Year	Type of duty
2025/2026	(N0719A270003) Nanotechnology	P	English	Ostrava	2	Compulsory	study plan
2024/2025	(N0719A270003) Nanotechnology	P	English	Ostrava	2	Compulsory	study plan
2023/2024	(N0719A270003) Nanotechnology	P	English	Ostrava	2	Compulsory	study plan
2022/2023	(N0719A270003) Nanotechnology	P	English	Ostrava	2	Compulsory	study plan
2021/2022	(N0719A270003) Nanotechnology	P	English	Ostrava	2	Compulsory	study plan
2020/2021	(N0719A270003) Nanotechnology	P	English	Ostrava	2	Compulsory	study plan
2019/2020	(N0719A270003) Nanotechnology	P	English	Ostrava	2	Compulsory	study plan

Occurrence in special blocks

Block name	Academic year	Form of study	Study language	Year	W	S	Type of block	Block owner

Assessment of instruction

Předmět neobsahuje žádné hodnocení.