9360-0185/01 – Laboratory Practice of Nanonaterials Preparation (LCPN)
Gurantor department | CNT - Nanotechnology Centre | Credits | 3 |
Subject guarantor | Ing. Karla Čech Barabaszová, Ph.D. Paed.IGIP | Subject version guarantor | Ing. Karla Čech Barabaszová, Ph.D. Paed.IGIP |
Study level | undergraduate or graduate | Requirement | Compulsory |
Year | 3 | Semester | winter |
| | Study language | Czech |
Year of introduction | 2019/2020 | Year of cancellation | |
Intended for the faculties | FMT, FEI, HGF, FS, FBI, FAST | Intended for study types | Bachelor |
Subject aims expressed by acquired skills and competences
To gain practical experience with the preparation of 1-3 dimensional nanotructured materials based on metals, metal oxides and sulphides of metals.
Teaching methods
Individual consultations
Experimental work in labs
Other activities
Summary
Laboratory exercises from the preparation of nanomaterials serve to practical acquaintance with methods of preparation of nanostructured materials based on metals, oxides and sulphides of metals. Students will focus on the methods of preparation from a solid and liquid environment within the blocks of laboratory exercises.
Compulsory literature:
Recommended literature:
Way of continuous check of knowledge in the course of semester
The student's knowledge of the given task is always checked at the beginning of the laboratory exercises in the form of a short test, and the student draws up a protocol from each laboratory exercise in which he answers the questions related to the respective task.
E-learning
Other requirements
For this subject are not the requirements for the student.
Prerequisities
Subject has no prerequisities.
Co-requisities
Subject has no co-requisities.
Subject syllabus:
1. Introductory tutorials. Introducing students to the lab, organizing laboratory exercises, safety and hygiene in laboratory work. Obligatory legal information to students about individual tasks, used chemicals and possible risks. Compilation of mandatory training documents.
Students work independently on the realization of laboratory tasks devoted to targeted preparation of nanostructured materials (see section 3-13). They use instrumentation, chemical reactants and chemical aids as specified in the protocol.
2. Ultrasonic synthesis of nanoparticles MgO.
3. Mechanochemical synthesis of CuO.
4. Preparation of Al2O3 particles by hydrolysis of AlCl3.
5. Solvothermal synthesis of ZnS nanoparticles.
6. Preparation of ZnO by the precipitation method.
7. Preparation of Ag nanoparticles by reaction with saccharides.
8. Preparation of CuO by microwave decomposition.
9. Preparation of magnetite by chemical precipitation reaction in liquids.
10. Preparation of ZnO nanoparticles by hydrothermal synthesis.
11. Roses - preparation of nanoparticles Ag.
12. Synthesis of CeO2 by precipitation from aqueous solution.
13. Chemical vapor deposition - preparation of 1 dimensional nanostructured materials.
14. Credit week. Replacement term The term is made by students who have missed the semester.
Conditions for subject completion
Occurrence in study plans
Occurrence in special blocks
Assessment of instruction