9360-0185/01 – Laboratory Practice of Nanonaterials Preparation (LCPN)

Gurantor departmentCNT - Nanotechnology CentreCredits3
Subject guarantorIng. Karla Čech Barabaszová, Ph.D. Paed.IGIPSubject version guarantorIng. Karla Čech Barabaszová, Ph.D. Paed.IGIP
Study levelundergraduate or graduateRequirementCompulsory
Year3Semesterwinter
Study languageCzech
Year of introduction2019/2020Year of cancellation
Intended for the facultiesFAST, FS, FBI, FEI, FMT, HGFIntended for study typesBachelor
Instruction secured by
LoginNameTuitorTeacher giving lectures
BAR31 Ing. Karla Čech Barabaszová, Ph.D. Paed.IGIP
HUN019 Ing. Marianna Hundáková, Ph.D.
STE17 Ing. Gabriela Kratošová, Ph.D.
Extent of instruction for forms of study
Form of studyWay of compl.Extent
Full-time Graded credit 0+3

Subject aims expressed by acquired skills and competences

To gain practical experience with the preparation of 1-3 dimensional nanotructured materials based on metals, metal oxides and sulphides of metals.

Teaching methods

Individual consultations
Experimental work in labs
Other activities

Summary

Laboratory exercises from the preparation of nanomaterials serve to practical acquaintance with methods of preparation of nanostructured materials based on metals, oxides and sulphides of metals. Students will focus on the methods of preparation from a solid and liquid environment within the blocks of laboratory exercises.

Compulsory literature:

SUGIMOTO, Tadao, ed. Fine Particles, Synthesis, Characterization and Mechanism of Growth. Marcel Dekker, New York, 2000. ISBN 0842700015. HOSOKAWA, Masuo, NAITO, Makio, YOKOYAMA, Toyokazu and Kiyoshi NOGI. Nanoparticle Technology Handbook. Elsevier, 2017. ISBN 9780444563682. BAUERLEIN, Edmund et. al, ed. Handbook of Biomineralization: Biological Aspects and Structure Formation. Wiley-VCH, 2009, ISBN 3527318054.4. RAO, C.N.R, ed. The Chemistry of Nanomaterials, Synthesis, Properties and Applications, Willey-VCH Weinheim, 2008. ISBN 3527306862.

Recommended literature:

RAI Mahendra and Clemens POSTEN. Green Biosynthesis of Nanoparticles - Mechanisms and Applications. CABI Publishing 2013, ISBN 9781780642239. Naito, Moto et. al, Nanoparticle Technology Handbook. Elsevier, 2017. ISBN 9780444563682. Nalwa H. S., editor. Encyclopedia of Nanoscience and Nanotechnology. Vol. 1-4. American Scientific Publisher, 2004. ISBN 1-58883-056-1.

Way of continuous check of knowledge in the course of semester

The student's knowledge of the given task is always checked at the beginning of the laboratory exercises in the form of a short test, and the student draws up a protocol from each laboratory exercise in which he answers the questions related to the respective task.

E-learning

Other requirements

For this subject are not the requirements for the student.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

1. Introductory tutorials. Introducing students to the lab, organizing laboratory exercises, safety and hygiene in laboratory work. Obligatory legal information to students about individual tasks, used chemicals and possible risks. Compilation of mandatory training documents. Students work independently on the realization of laboratory tasks devoted to targeted preparation of nanostructured materials (see section 3-13). They use instrumentation, chemical reactants and chemical aids as specified in the protocol. 2. Ultrasonic synthesis of nanoparticles MgO. 3. Mechanochemical synthesis of CuO. 4. Preparation of Al2O3 particles by hydrolysis of AlCl3. 5. Solvothermal synthesis of ZnS nanoparticles. 6. Preparation of ZnO by the precipitation method. 7. Preparation of Ag nanoparticles by reaction with saccharides. 8. Preparation of CuO by microwave decomposition. 9. Preparation of magnetite by chemical precipitation reaction in liquids. 10. Preparation of ZnO nanoparticles by hydrothermal synthesis. 11. Roses - preparation of nanoparticles Ag. 12. Synthesis of CeO2 by precipitation from aqueous solution. 13. Chemical vapor deposition - preparation of 1 dimensional nanostructured materials. 14. Credit week. Replacement term The term is made by students who have missed the semester.

Conditions for subject completion

Full-time form (validity from: 2019/2020 Winter semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of points
Graded credit Graded credit 100 (100) 51
        Laboratorní protokoly Laboratory work 80  50
        Test Written test 20  12
Mandatory attendence parzicipation: Laboratory work

Show history

Occurrence in study plans

Academic yearProgrammeField of studySpec.ZaměřeníFormStudy language Tut. centreYearWSType of duty
2021/2022 (B0719A270001) Nanotechnology P Czech Ostrava 3 Compulsory study plan
2020/2021 (B0719A270001) Nanotechnology P Czech Ostrava 3 Compulsory study plan
2019/2020 (B0719A270001) Nanotechnology P Czech Ostrava 3 Compulsory study plan

Occurrence in special blocks

Block nameAcademic yearForm of studyStudy language YearWSType of blockBlock owner