9360-0207/01 – Methods of organic analysis for characterization of nanostructured materials (MOA)

Gurantor departmentCNT - Nanotechnology CentreCredits10
Subject guarantordoc. Ing. Daniela Plachá, Ph.D.Subject version guarantordoc. Ing. Daniela Plachá, Ph.D.
Study levelpostgraduateRequirementChoice-compulsory
YearSemesterwinter + summer
Study languageCzech
Year of introduction2012/2013Year of cancellation
Intended for the facultiesUSPIntended for study typesDoctoral
Instruction secured by
LoginNameTuitorTeacher giving lectures
PLA88 doc. Ing. Daniela Plachá, Ph.D.
Extent of instruction for forms of study
Form of studyWay of compl.Extent
Full-time Examination 0+0
Combined Examination 0+0

Subject aims expressed by acquired skills and competences

The aim of this subject is deepening of knowledge in the sphere of analytical methods for qualitative and quantitative organic analysis that are applied for characterization and testing of effectivity of nanostructured materials (sorbents, catalysts), nanomaterials with antibacterial effects and observation of interaction of nanostructured materials and nanoparticles with other materials such as organic compounds, biological tissues and others.

Teaching methods

Individual consultations
Experimental work in labs

Summary

The aim of this subject is deepening of knowledge in the sphere of analytical methods for qualitative and quantitative organic analysis that are applied for characterization and testing of effectivity of nanostructured materials (sorbents, catalysts), nanomaterials with antibacterial effects and observation of interaction of nanostructured materials and nanoparticles with other materials such as organic compounds, biological tissues and others. The first part is aimed to study of chromatografic methods in connection with mass detectors GC/MS, GC/MSn, LC/MS, LC/MSn and utilization of gel permeation chromatografy. Attention will be aimed to advanced spectroscopic methods: NMR, high resolution ESR, FTIR and Raman spectrometry, mass spectrometry and possibilities of their application. The second part is aimed to practical exercises with chromatografic and spectroscopic reports to deepen students abilities to work with mentioned methods. Student will get basic skills for work with real chromatographic and spectroscopic data sets. Third part is aimed to practical preparation and optimalization of analytical methods for deepening his knowledge in the sphere of performing of analysis with quality results assurance and keeping of principle of good laboratory practise. Student will get skills for sample preparations and their analysis so that he will be able produce high-quality and reliable data sets, including of abilitity to perform method validation and calculate measurement uncertainety, especially for chromatografic methods.

Compulsory literature:

H. J. Hübschmann, Handbook of GC/MS (Sec. Ed.), Wiley-VCH Verlag GmbH & Co., KGaA, Weinheim 2008. ISBN 978-3-527-31427-0. 2. M. C. McMaster, LC/MS, John Wiley&Sons, New York 2005. ISBN 978-047-16553-12. 3. G. Gauglitz, T. Vo-Dinh, Handbook of Spectroscopy, Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim 2005. ISBN 978-3-527-29782-5. 4. J. D. Winefordner, Sample Preparation Techniques in Analytical Chemistry, Volume 162, John Wiley & Sons, Inc. 2003. ISBN 0-471-32845-6.

Recommended literature:

M. C. Mc Master, GC/MS (Sec. Ed.), John Wiley & Sons, Inc. Hoboken, NJ, USA 2007. ISBN 978-047-010163-6. 2. S. Wartewig, IR and Raman Spectroscopy: Fundamental Processing, VCH Verlag GmbH & Co. KGaA, Weinheim 2003. ISBN 3-527-30245-X. 3. R. G. Brereton, Applied Chemometrics for Scientists, John Wiley & Sons, New York 2007. ISBN 9780470016862.

Way of continuous check of knowledge in the course of semester

E-learning

Další požadavky na studenta

For this subject other requirements for student are not determined.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

1. Chromatographic methods, mass spectrometry. 2. Coupling of chromatographic methods with mass spectrometry, applications. 3. Spectroscopic methods for organic analysis, IR and Raman spectroscopy, applications. 4. Nuclear magnetic resonance and electron paramagnetic resonance, aplications. 5. Evaluation of chromatographic results. 6. Evaluation of mass spectra. 7. Basic principles and procedures for evaluation of IR spectra. 8. Basic principles and procedures for evaluation of Raman spectra. 9. Basic principles and procedures for evaluation of NMR spectra. 10. Basic principles and procedures for evaluation of EPR (ESR) spectra. 11. Preparation and development of analytical method for organic analysis. 12. Validation of method. 13. Measurement uncertainety. 14. Basic of Good laboratory Practise (GLP) and Quality Management in analytical laboratory.

Conditions for subject completion

Full-time form (validity from: 2013/2014 Winter semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of points
Examination Examination  
Mandatory attendence parzicipation:

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Occurrence in study plans

Academic yearProgrammeField of studySpec.FormStudy language Tut. centreYearWSType of duty
2019/2020 (P3942) Nanotechnology (3942V001) Nanotechnology P Czech Ostrava Choice-compulsory study plan
2019/2020 (P3942) Nanotechnology (3942V001) Nanotechnology K Czech Ostrava Choice-compulsory study plan
2018/2019 (P3942) Nanotechnology (3942V001) Nanotechnology P Czech Ostrava Choice-compulsory study plan
2018/2019 (P3942) Nanotechnology (3942V001) Nanotechnology K Czech Ostrava Choice-compulsory study plan
2017/2018 (P3942) Nanotechnology (3942V001) Nanotechnology P Czech Ostrava Choice-compulsory study plan
2017/2018 (P3942) Nanotechnology K Czech Ostrava Choice-compulsory study plan
2017/2018 (P3942) Nanotechnology (3942V001) Nanotechnology K Czech Ostrava Choice-compulsory study plan
2016/2017 (P3942) Nanotechnology (3942V001) Nanotechnology P Czech Ostrava Choice-compulsory study plan
2016/2017 (P3942) Nanotechnology (3942V001) Nanotechnology K Czech Ostrava Choice-compulsory study plan
2015/2016 (P3942) Nanotechnology (3942V001) Nanotechnology P Czech Ostrava Choice-compulsory study plan
2015/2016 (P3942) Nanotechnology (3942V001) Nanotechnology K Czech Ostrava Choice-compulsory study plan
2014/2015 (P3942) Nanotechnology (3942V001) Nanotechnology P Czech Ostrava Choice-compulsory study plan
2014/2015 (P3942) Nanotechnology P Czech Ostrava Choice-compulsory study plan
2014/2015 (P3942) Nanotechnology (3942V001) Nanotechnology K Czech Ostrava Choice-compulsory study plan
2013/2014 (P3942) Nanotechnology (3942V001) Nanotechnology P Czech Ostrava Choice-compulsory study plan
2013/2014 (P3942) Nanotechnology (3942V001) Nanotechnology K Czech Ostrava Choice-compulsory study plan
2012/2013 (P3942) Nanotechnology (3942V001) Nanotechnology P Czech Ostrava Choice-compulsory study plan
2012/2013 (P3942) Nanotechnology (3942V001) Nanotechnology K Czech Ostrava Choice-compulsory study plan

Occurrence in special blocks

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