9360-0207/01 – Methods of organic analysis for characterization of nanostructured materials (MOA)
Gurantor department | CNT - Nanotechnology Centre | Credits | 10 |
Subject guarantor | prof. Ing. Daniela Plachá, Ph.D. | Subject version guarantor | prof. Ing. Daniela Plachá, Ph.D. |
Study level | postgraduate | Requirement | Choice-compulsory |
Year | | Semester | winter + summer |
| | Study language | Czech |
Year of introduction | 2012/2013 | Year of cancellation | |
Intended for the faculties | USP, HGF | Intended for study types | Doctoral |
Subject aims expressed by acquired skills and competences
The aim of this subject is deepening of knowledge in the sphere of analytical methods for qualitative and quantitative organic analysis that are applied for characterization and testing of effectivity of nanostructured materials (sorbents, catalysts), nanomaterials with antibacterial effects and observation of interaction of nanostructured materials and nanoparticles with other materials such as organic compounds, biological tissues and others.
Teaching methods
Individual consultations
Experimental work in labs
Summary
The aim of this subject is deepening of knowledge in the sphere of analytical methods for qualitative and quantitative organic analysis that are applied for characterization and testing of effectivity of nanostructured materials (sorbents, catalysts), nanomaterials with antibacterial effects and observation of interaction of nanostructured materials and nanoparticles with other materials such as organic compounds, biological tissues and others.
The first part is aimed to study of chromatografic methods in connection with mass detectors GC/MS, GC/MSn, LC/MS, LC/MSn and utilization of gel permeation chromatografy. Attention will be aimed to advanced spectroscopic methods: NMR, high resolution ESR, FTIR and Raman spectrometry, mass spectrometry and possibilities of their application.
The second part is aimed to practical exercises with chromatografic and spectroscopic reports to deepen students abilities to work with mentioned methods. Student will get basic skills for work with real chromatographic and spectroscopic data sets.
Third part is aimed to practical preparation and optimalization of analytical methods for deepening his knowledge in the sphere of performing of analysis with quality results assurance and keeping of principle of good laboratory practise. Student will get skills for sample preparations and their analysis so that he will be able produce high-quality and reliable data sets, including of abilitity to perform method validation and calculate measurement uncertainety, especially for chromatografic methods.
Compulsory literature:
Recommended literature:
Way of continuous check of knowledge in the course of semester
Individual consultations, oral exam.
E-learning
Other requirements
For this subject other requirements for student are not determined.
Prerequisities
Subject has no prerequisities.
Co-requisities
Subject has no co-requisities.
Subject syllabus:
Chromatographic methods, mass spectrometry.
Coupling of chromatographic methods with mass spectrometry, applications.
Spectroscopic methods for organic analysis, IR and Raman spectroscopy, applications.
Nuclear magnetic resonance and electron paramagnetic resonance, aplications.
Evaluation of chromatographic results.
Evaluation of mass spectra.
Basic principles and procedures for evaluation of IR spectra.
Basic principles and procedures for evaluation of Raman spectra.
Basic principles and procedures for evaluation of NMR spectra.
Basic principles and procedures for evaluation of EPR (ESR) spectra.
Preparation and development of analytical method for organic analysis.
Validation of method, measurement uncertainety.
Basic of Good laboratory Practise (GLP) and Quality Management in analytical laboratory.
Conditions for subject completion
Occurrence in study plans
Occurrence in special blocks
Assessment of instruction
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