9360-0211/01 – Special Methods of Analytical Chemistry (SMACH)

Gurantor departmentCNT - Nanotechnology CentreCredits10
Subject guarantordoc. Ing. Vladimír Tomášek, CSc.Subject version guarantordoc. Ing. Vladimír Tomášek, CSc.
Study levelpostgraduateRequirementChoice-compulsory
YearSemesterwinter + summer
Study languageCzech
Year of introduction2012/2013Year of cancellation
Intended for the facultiesUSPIntended for study typesDoctoral
Instruction secured by
LoginNameTuitorTeacher giving lectures
TOM24 doc. Ing. Vladimír Tomášek, CSc.
Extent of instruction for forms of study
Form of studyWay of compl.Extent
Full-time Examination 0+0
Combined Examination 0+0

Subject aims expressed by acquired skills and competences

Students become more familiar with the methods of chemical analysis of materials with a focus on the analysis of nanomaterials. Attention will be paid to the chosen spectral methods. Methods of X-ray spectral analysis, electron spectroscopy and emission spectral analysis with glow discharge for the analysis of very thin layers will be discussed. There will also be introduced to methods of spectral analysis in combination with electron microscopes and Raman spectroscopy in combination with a microscope.

Teaching methods

Individual consultations

Summary

Compulsory literature:

1. J. Kenkel, Analytical Chemistry for Technicians, Third Edition, CRC 2002. 2. R. Tertian, F. Claisse, Priciples of Quantitative X-Ray Fluorescence Analysis, Hayden & son Ltd, London 1982.

Recommended literature:

1. E. P. Bertin, Principles and Practice of X-Ray Spectrometric Analysis, Plenum Press, New York - London 1975. 2. D. B. Williams, Practical Analytical Electron Microscopy in Materials Science, Verlag chemie international, Florida - Basel 1984. 3. N. Yao, Z. L. Wang (Eds.), Handbook of microscopy for nanotechnology, Kluwer Acadenic Publishers, Boston 2005.

Way of continuous check of knowledge in the course of semester

E-learning

Další požadavky na studenta

Write a seminar work. Topic of the seminar work is defined by supervisor.

Prerequisities

Subject has no prerequisities.

Co-requisities

Subject has no co-requisities.

Subject syllabus:

1. Spectral methods of analytical chemistry Atomic emission spectrometry (excitation by spark, glow discharge, ICP), optical spectrometry, mass spectrometry Atomic absorption spectrometry (flame and electro thermal atomization, gaseous hydrides method) X-ray spectral analysis, X-ray fluorescence spectrometry (XRF), XRF with focused X-ray beam, total reflection method, grazing method Electron spectroscopy (XPS, AES) Molecular absorption analysis, UV/VIS spectrometry, infrared spectrometry, Raman spectrometry, Raman microscopy 2. Electrochemical methods. Conductometry, conductometric titrations Potentiometry, ion selective electrodes, potentiometric titration Electrolytical methods, voltammetry (polarography), new voltammetric methods, coulometry Electromigration separation methods, capillary electrophoresis, isotachophoresis 3. Analytical electron microscopy (AEM) Basics of electron microscopy, interaction of electron beam with matter and basic components of electron microscopes Transmition electron microscopy (TEM), scanning electron microscopy (SEM), scanning transmition electron microscopy (STEM) X-ray spectral microanalysis, Auger electrons spectrometry Electron energy loss spectrometry (EELS) Focused ion beam (FIB), manipulation with sample in nano - scale

Conditions for subject completion

Full-time form (validity from: 2013/2014 Winter semester)
Task nameType of taskMax. number of points
(act. for subtasks)
Min. number of points
Examination Examination  
Mandatory attendence parzicipation:

Show history

Occurrence in study plans

Academic yearProgrammeField of studySpec.FormStudy language Tut. centreYearWSType of duty
2019/2020 (P3942) Nanotechnology (3942V001) Nanotechnology P Czech Ostrava Choice-compulsory study plan
2019/2020 (P3942) Nanotechnology (3942V001) Nanotechnology K Czech Ostrava Choice-compulsory study plan
2018/2019 (P3942) Nanotechnology (3942V001) Nanotechnology P Czech Ostrava Choice-compulsory study plan
2018/2019 (P3942) Nanotechnology (3942V001) Nanotechnology K Czech Ostrava Choice-compulsory study plan
2017/2018 (P3942) Nanotechnology (3942V001) Nanotechnology P Czech Ostrava Choice-compulsory study plan
2017/2018 (P3942) Nanotechnology K Czech Ostrava Choice-compulsory study plan
2017/2018 (P3942) Nanotechnology (3942V001) Nanotechnology K Czech Ostrava Choice-compulsory study plan
2016/2017 (P3942) Nanotechnology (3942V001) Nanotechnology P Czech Ostrava Choice-compulsory study plan
2016/2017 (P3942) Nanotechnology (3942V001) Nanotechnology K Czech Ostrava Choice-compulsory study plan
2015/2016 (P3942) Nanotechnology (3942V001) Nanotechnology P Czech Ostrava Choice-compulsory study plan
2015/2016 (P3942) Nanotechnology (3942V001) Nanotechnology K Czech Ostrava Choice-compulsory study plan
2014/2015 (P3942) Nanotechnology (3942V001) Nanotechnology P Czech Ostrava Choice-compulsory study plan
2014/2015 (P3942) Nanotechnology P Czech Ostrava Choice-compulsory study plan
2014/2015 (P3942) Nanotechnology (3942V001) Nanotechnology K Czech Ostrava Choice-compulsory study plan
2013/2014 (P3942) Nanotechnology (3942V001) Nanotechnology P Czech Ostrava Choice-compulsory study plan
2013/2014 (P3942) Nanotechnology (3942V001) Nanotechnology K Czech Ostrava Choice-compulsory study plan
2012/2013 (P3942) Nanotechnology (3942V001) Nanotechnology P Czech Ostrava Choice-compulsory study plan
2012/2013 (P3942) Nanotechnology (3942V001) Nanotechnology K Czech Ostrava Choice-compulsory study plan

Occurrence in special blocks

Block nameAcademic yearForm of studyStudy language YearWSType of blockBlock owner