9360-0227/01 – Characterization methods of nanostructures (MCHN)
| Gurantor department | CNT - Nanotechnology Centre | Credits | 10 |
| Subject guarantor | doc. Dr. Mgr. Kamil Postava | Subject version guarantor | doc. Dr. Mgr. Kamil Postava |
| Study level | postgraduate | Requirement | Compulsory |
| Year | | Semester | winter + summer |
| | Study language | Czech |
| Year of introduction | 2020/2021 | Year of cancellation | |
| Intended for the faculties | FMT | Intended for study types | Doctoral |
Subject aims expressed by acquired skills and competences
The main target of the subject is to obtain overview of characterization methods for study of nanostructures. Particular target is deep understanding and detail practicing of the characterization methods relating to the subject of thesis of the student.
Teaching methods
Lectures
Individual consultations
Experimental work in labs
Summary
The subject includes physical and chemical characterization methods for nanostructures, measurement principles, limits of different techniques, and specific applications. Focus of the subject will be chosen in agreement with specialization of the student and title of his thesis.
Compulsory literature:
S. Myhra, J. C. Rivière, Characterization of Nanostructures, CRC Press 2016
D.Brabazon and A.Raffer, Advanced Characterization Techniques for Nanostructures, In: Emerging Nanotechnologies for Manufacturing, Edited by: W. Ahmed and M. J. Jackson, William Andrew Publ. 2009
A. L. Da Róz, M. Ferreira, O. N. Oliveira, Jr., Nanocharacterization Techniques, 2017
S. T. Raju, T, Ajesh Z. R. Kumar, Microscopy Methods in Nanomaterials Characterization, Elsevier 2017
R. Haight, J. B Hannon, Handbook of Instrumentation and Techniques for Semiconductor Nanostructure Characterization, World Scientific 2011
E. Lundanes, L. Reubsaet, T. Greibrokk, Chromatography, basic Principles, Sample Preparations and Related Methods, J. Wiley and Sons, 2014
Recommended literature:
B. Bhushan (Ed.), Scanning Probe Microscopy in Nanoscience and Nanotechnology, Sprnger 2010
B. Voigtländer, Scanning Probe Microscopy: Atomic Force Microscopy and Scanning Tunneling Microscopy (NanoScience and Technology), Springer 2015
S. Svanberg, Atomic and molecular spectroscopy: basic aspects and practical applications, Springer-Verlag, Berlin 1991
P. Griffiths, J. A. De Haseth, Fourier Transform Infrared Spectrometry (Chemical Analysis: A Series of Monographs on Analytical Chemistry and Its Applications), Wiley 2nd. Ed, 2007
N. Yao, Z. L. Wang, Handbook of Microscopy for Nanotechnology (Nanostructure Science and TX‐Rays in Nanoscience: Spectroscopy, Spectromicroscopy, and Scattering Techniquesechnology), Springer 2005
J. Guo, X‐Rays in Nanoscience: Spectroscopy, Spectromicroscopy, and Scattering Techniques, Willey 2010
M. F. Vitha, Chromatography: Principles and Instrumentation, J. Wiley and Sons, 2017
Way of continuous check of knowledge in the course of semester
oral exam
E-learning
Other requirements
The main target of the subject is to obtain overview of characterization methods for study of nanostructures. Particular target is deep understanding and detail practicing of the characterization methods relating to the subject of thesis of the student.
Prerequisities
Subject has no prerequisities.
Co-requisities
Subject has no co-requisities.
Subject syllabus:
1. Electron microscopy of nanostructures (sample preparation, Scanning Electron Microscopy, Transmission Electron Microscopy, special methods of electron microscopy)
2. Scanning probe microscopy (Atomic Force Microscopy, Magnetic Force Microscopy, Scanning Near-field Optical Microscopy, Scanning Tunelling Microscopy)
3. X-ray spectroscopy and diffraction (X-ray diffraction, X-ray Photoeelectron Spectroscopy, Energy Dispersive X-ray Spectroscopy)
4. Optical spectroscopy of nanostructures (ultraviolet, visible spektroscopy, photoluminiscence, Fourier Transform InfraRed spectroscopy, THz spectroscopy, Raman spektroscopy, Atomic Absorption Spectroscopy), Inductively Coupled Plasma Spectroscopy, Mass Spectrometry, Nuclear Magnetic Resonance
5. Thermal analysis (Differential Thermal Analysis, Differential Scanning Calorimetry, Thermogravimetric analysis, simultaneous TG/DTA/DSC)
6. Measurement of size and shape of nanoparticles, and surface porosity (Laser diffraction, chromatography, Dynamic Light Scattering)
7. Organic analysis for nanostructure characterization (size exclusion chromatography, supercritical fluid, gas, liquid chromatography, mass detectors in chromatography, electromigration methods)
Conditions for subject completion
Occurrence in study plans
Occurrence in special blocks
Assessment of instruction
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