9360-0229/01 – Special Methods of Analytical Chemistry (SMACH)
| Gurantor department | CNT - Nanotechnology Centre | Credits | 10 |
| Subject guarantor | prof. Ing. Jana Seidlerová, CSc. | Subject version guarantor | prof. Ing. Jana Seidlerová, CSc. |
| Study level | postgraduate | Requirement | Choice-compulsory type B |
| Year | | Semester | winter + summer |
| | Study language | Czech |
| Year of introduction | 2019/2020 | Year of cancellation | |
| Intended for the faculties | FMT | Intended for study types | Doctoral |
Subject aims expressed by acquired skills and competences
The aim of the course is focused on methods of inorganic analysis of nanomaterials. Particular attention will be paid to the selected spectral methods such as X-ray spectral analysis, absorption and emission methods in both ultraviolet and visible spectrum, methods used for chemical analysis of thin films and direct chemical analysis of micro/nano particles.
Teaching methods
Individual consultations
Project work
Summary
The course is focused on methods of inorganic analysis of nanomaterials. Particular attention will be paid to the selected spectral methods such as X-ray spectral analysis, absorption and emission methods in both ultraviolet and visible spectrum, methods used for chemical analysis of thin films and direct chemical analysis of micro/nano particles. The mentioned methods will be supplemented with an overview of modern sophisticated methods combinations such as electron microscope and the Raman spectroscopy, electon microscope and the X-ray or electron diffraction spectroscopy. Analytical chemistry utilising nanomaterials will be also introduced in a part of the course.
Compulsory literature:
Recommended literature:
Way of continuous check of knowledge in the course of semester
Zpracování seminární práce na zadané téma v min rozsahu 5 stran formátu A4, ústní zkouška.
E-learning
Other requirements
Write a seminar work. Topic of the seminar work is defined by supervisor.
Prerequisities
Subject has no prerequisities.
Co-requisities
Subject has no co-requisities.
Subject syllabus:
1. Spectral methods of analytical chemistry
Atomic emission spectrometry (excitation by spark, glow discharge, ICP), optical spectrometry, mass spectrometry
Atomic absorption spectrometry (flame and electro thermal atomization, gaseous hydrides method)
X-ray spectral analysis, X-ray fluorescence spectrometry (XRF), XRF with focused X-ray beam, total reflection method, grazing method
Electron spectroscopy (XPS, AES)
Molecular absorption analysis, UV/VIS spectrometry, infrared spectrometry, Raman spectrometry, Raman microscopy
2. Electrochemical methods
Conductometry, conductometric titrations
Potentiometry, ion selective electrodes, potentiometric titration
Electrolytical methods, voltammetry (polarography), new voltammetric methods, coulometry
Electromigration separation methods, capillary electrophoresis, isotachophoresis
3. Analytical electron microscopy (AEM)
Basics of electron microscopy, interaction of electron beam with matter and basic components of electron microscopes
Transmition electron microscopy (TEM), scanning electron microscopy (SEM), scanning transmition electron microscopy (STEM)
X-ray spectral microanalysis, Auger electrons spectrometry
Electron energy loss spectrometry (EELS)
Focused ion beam (FIB), manipulation with sample in nano - scale
Conditions for subject completion
Occurrence in study plans
Occurrence in special blocks
Assessment of instruction
Předmět neobsahuje žádné hodnocení.